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  • 1
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: The size of the crystalline regions of regenerated cellulosic fibers was determined by means of transmission electron microscopy, small angle X-ray scattering, and wide angle X-ray diffraction. All three methods lead in satisfying conformity to the following dimensions: length: 120-140 Å, width: 80-100 Å, thickness: 30-40 Å. The broad plane of the platelet shaped crystallites is situated parallel to the 101-lattice plane, the small edge plane has an orientation parallel to the 101-lattice plane. The -crystallites form strands, which have a length of 1500-5500 Å. They are partly bundled up to clusters with a diameter of 300-600 Å, partly separated by less dense spacings. The distance between the crystalline regions amounts to 20-40 Å in longitudinal and cross direction.
    Notes: Die Dimensionen der kristallinen Bereiche von Regeneratcellulosefasern wurden mittels Transmissionselektronenmikroskopie, Röntgenkleinwinkelstreuung und Röntgenweitwinkeldiffraktion bestimmt. In befriedigender Übereinstimmung wurden nach allen drei Methoden folgende Abmessungen gefunden: Länge: 120-140 Å, Breite: 80-100 Å, Dicke: 30-40 Å. Die breite Ebene der blättchenförmigen Kristallite verläuft parallel zur 101-Netzebene, die schmale Kantenebene parallel zur 101-Netzebene. Die Kristallite bilden Ketten mit einer Länge von 1500 bis 5500 Å, die teilweise zu Clustern mit einem Durchmesser von 300 bis 600 Å gebündelt sind, teilweise durch Zonen geringerer Dichte voneinander getrennt sind. Die Abstände zwischen den kristallinen Bereichen betragen in Längs- und Querrichtung 20 bis 40 Å.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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