Online Resource
Singapore :Springer Singapore Pte. Limited,
Keywords:
Electronic books.
Type of Medium:
Online Resource
Pages:
1 online resource (267 pages)
Edition:
1st ed.
ISBN:
9789811369674
Series Statement:
Lecture Notes in Chemistry Series ; v.103
URL:
https://ebookcentral.proquest.com/lib/geomar/detail.action?docID=5771924
Language:
English
Note:
Intro -- Preface -- Contents -- 1 Solid-State NMR Principles and Techniques -- 1.1 Introduction -- 1.2 Nuclear Spin Interactions in Solids -- 1.2.1 Chemical Shift Interaction -- 1.2.2 Dipole-Dipole Interaction -- 1.2.3 Quadrupolar Interaction -- 1.2.4 Spin-Spin Interaction -- 1.3 Manipulations of Spin Interactions in Solids -- 1.3.1 Magic-Angle Spinning (MAS) -- 1.3.2 Cross-Polarization -- 1.3.3 Dipolar Decoupling Methods in Rotating Solid -- 1.3.4 Dipolar Recoupling Methods in Rotating Solid -- 1.3.5 High-Resolution Techniques for Half-Integer-Spin Quadrupolar Nuclei -- 1.3.6 Summary -- References -- 2 Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis -- 2.1 Introduction -- 2.2 Zeolite Synthesis Route and Procedures -- 2.3 Zeolite Synthesis Process and Crystallization Mechanism -- 2.4 NMR Strategy in Characterization of Zeolite Synthesis -- 2.4.1 Microporous Aluminosilicates -- 2.4.2 Microporous Aluminophosphates -- 2.5 Summary -- References -- 3 Solid-State NMR Characterization of Framework Structure of Zeolites and Zeotype Materials -- 3.1 Introduction -- 3.2 Solid-State NMR Characterization of Zeolite Framework Structure -- 3.2.1 27Al MAS NMR -- 3.2.2 29Si MAS NMR -- 3.2.3 31P MAS NMR -- 3.2.4 17O MAS NMR -- 3.2.5 129Xe NMR -- 3.2.6 Other Framework Elements -- 3.3 Summary -- References -- 4 Solid-State NMR Characterization of Host-Guest Interactions -- 4.1 Introduction -- 4.2 Solid-State NMR Characterization of Host-Guest Interactions -- 4.2.1 Host-Guest Interaction Between Adsorbed Molecule and Zeolite Framework -- 4.2.2 Host-Guest Interaction in Molecular Sieve Synthesis -- 4.2.3 Host-Guest Interaction in Zeolite Catalysis -- 4.3 Summary -- References -- 5 Solid-State NMR Characterization of Acid Properties of Zeolites and Solid Acid Catalysts -- 5.1 Introduction -- 5.2 Solid-State NMR Characterization of Acidic Property.
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5.2.1 Acid Sites Containing Hydroxyl Groups -- 5.2.2 Acidic Nature and Strength -- 5.2.3 Location and Distribution of Acid Sites -- 5.2.4 Spatial Proximities and Synergy Effects of Different Acid Sites -- 5.3 Summary -- References -- 6 In Situ Solid-State NMR Investigation of Catalytic Reactions on Zeolites -- 6.1 Introduction -- 6.2 In Situ Solid-State NMR Approaches -- 6.2.1 Batch Reaction -- 6.2.2 Flow Reaction -- 6.3 Mechanistic Study of the Catalytic Reactions by In Situ NMR -- 6.3.1 Activation and Conversion of Light Alkanes -- 6.3.2 Methanol-to-Olefins (MTO) Conversion -- 6.4 Summary -- References -- Index.
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