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  • 1
    Keywords: Forschungsbericht ; Ressourceneffizienz
    Type of Medium: Online Resource
    Pages: 1 Online-Ressource (5 Seiten, 407,80 KB)
    Language: German
    Note: Förderkennzeichen BMBF 031B0432 , Unterschiede zwischen dem gedruckten Dokument und der elektronischen Ressource können nicht ausgeschlossen werden
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  • 2
    Keywords: Forschungsbericht ; Biotopverbund ; Ökosystemdienstleistung
    Type of Medium: Online Resource
    Pages: 1 Online-Ressource (16 Seiten, 2,00 MB) , Diagramme
    Language: German
    Note: Förderkennzeichen BMBF 16LC1611B [neu] - 01LC1611B [alt] , Verbundnummer 01176530 , Unterschiede zwischen dem gedruckten Dokument und der elektronischen Ressource können nicht ausgeschlossen werden , Sprache der Zusammenfassung: Deutsch, Englisch
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  • 3
    Publication Date: 2023-01-21
    Description: The study took place in Schleswig-Holstein, Northern Germany, in spring 2019. We have chosen 15 arable fields that are part of the federal soil monitoring scheme by LLUR and as such are representative of the different soil conditions in the region. At each of the 15 study fields, boreholes were placed along the corner points of a square of approximately 40 m edge length. At each of the corner points, three boreholes were drilled down to depths of 10, 20 and 30 cm, respectively. As a consequence, we had 4 x 3 x 3 = 36 sampling units with a wet weight of ~ 200 g soil per unit that integrated over soil depths of 0-10 cm, 10-20 cm and 20-30 cm, respectively, per study site. Each sampling unit was dimensioned with a ruler and stored in an individual glass container (Figure 1). Thus, in this study a total of 540 sampling units with a total of 123.3 kg soil material was inspected for plastic particles between 1 and 5 mm. In the laboratory, the wet soil mass of each sampling unit was quantified and then the soil volume was reduced by wet sieving. To facilitate the sieving, the soil was first soaked in lukewarm tap water in a beaker (1 l) to dissolve loamy aggregates. Aggregates that did not dissolve easily were gently broken down with the fingers and carefully homogenized with a metal whisk. Then the soil was placed on a steel analysis sieve with a mesh size of 1 mm and rinsed under running tap water until only particles of 〉 1 mm remained. This material was then transferred into glass petri dishes by using a squeeze bottle made of Polyethylene (PE) filled with tap water and a metal spoon. Excess water was removed from the petri dishes with a disposable syringe (PE and Polypropylene (PP)) and an attached injection cannula (outer diameter 0.8 mm; PP and metal) (Figure 1). Next, the content of each petri dish was visually examined twice (once by IK Harms and once by S Troegel) for MP under a stereomicroscope with transmitted light and a 133 Trino Zoom (BMS) with two WF 10x/22 mm oculars. All particles that matched the criteria for the proper identification of MP recommended by Hidalgo-Ruz et al. (2012) were picked and individually placed in 96-well micro test plates that were made from Polystyrene (PS). For their unambiguous identification the sorted particles were analysed with a Fourier transform infrared (FTIR) spectrometer model Spectrum Two™ by PerkinElmer Inc. For the identification of the polymer type, the particles were placed individually on a diamond-/ZnSe crystal plate and eight scans per particle were performed at room temperature with a resolution of 4 cm-1 each. The measured spectrum was then automatically compared with the known spectra of thousands of specific substances stored in a reference library of the PerkinElmer SpectrumTM10 ES software.
    Keywords: Farmland; Ploughing; Polymertype; Quantification; Terrestrial Pollution; Topsoil
    Type: Dataset
    Format: application/zip, 3 datasets
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  • 4
    Publication Date: 2023-01-21
    Description: To assure the reliability and efficiency of the method we conducted a recovery experiment. For this purpose, we spiked 8 soil samples in a way that each contained 20 particles between 1-5 mm. These were 5 black foils (PE), 5 black fragments (PP), 5 white/green platelets (PE) and 5 fibres (PA). We processed the samples according to the method described above, and inspected them twice. Recovery success was 93%, while samples with high organic content in particular impaired the recovery of fibres.
    Keywords: Experiment; Farmland; Observation; Plastic particles; Ploughing; Polymertype; Quantification; Recovery; Sample ID; Terrestrial Pollution; Topsoil
    Type: Dataset
    Format: text/tab-separated-values, 128 data points
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  • 5
    Publication Date: 2023-02-07
    Description: The study took place in Schleswig-Holstein, Northern Germany, in spring 2019. We have chosen 15 arable fields that are part of the federal soil monitoring scheme by LLUR and as such are representative of the different soil conditions in the region. At each of the 15 study fields, boreholes were placed along the corner points of a square of approximately 40 m edge length. At each of the corner points, three boreholes were drilled down to depths of 10, 20 and 30 cm, respectively. As a consequence, we had 4 x 3 x 3 = 36 sampling units with a wet weight of ~ 200 g soil per unit that integrated over soil depths of 0-10 cm, 10-20 cm and 20-30 cm, respectively, per study site. Each sampling unit was dimensioned with a ruler and stored in an individual glass container. Thus, in this study a total of 540 sampling units with a total of 123.3 kg soil material was inspected for plastic particles between 1 and 5 mm. In the laboratory, the wet soil mass of each sampling unit was quantified and then the soil volume was reduced by wet sieving. To facilitate the sieving, the soil was first soaked in lukewarm tap water in a beaker (1 l) to dissolve loamy aggregates. Aggregates that did not dissolve easily were gently broken down with the fingers and carefully homogenized with a metal whisk. Then the soil was placed on a steel analysis sieve with a mesh size of 1 mm and rinsed under running tap water until only particles of 〉 1 mm remained. This material was then transferred into glass petri dishes by using a squeeze bottle made of Polyethylene (PE) filled with tap water and a metal spoon. Excess water was removed from the petri dishes with a disposable syringe (PE and Polypropylene (PP)) and an attached injection cannula (outer diameter 0.8 mm; PP and metal). Next, the content of each petri dish was visually examined twice (once by IK Harms and once by S Troegel) for MP under a stereomicroscope with transmitted light and a 133 Trino Zoom (BMS) with two WF 10x/22 mm oculars. All particles that matched the criteria for the proper identification of MP recommended by Hidalgo-Ruz et al. (2012) were picked and individually placed in 96-well micro test plates that were made from Polystyrene (PS). For their unambiguous identification the sorted particles were analysed with a Fourier transform infrared (FTIR) spectrometer model Spectrum Two™ by PerkinElmer Inc. For the identification of the polymer type, the particles were placed individually on a diamond-/ZnSe crystal plate and eight scans per particle were performed at room temperature with a resolution of 4 cm-1 each. The measured spectrum was then automatically compared with the known spectra of thousands of specific substances stored in a reference library of the PerkinElmer SpectrumTM10 ES software.
    Keywords: Color description; Correlation; DEPTH, sediment/rock; Depth comment; Farmland; Identification; Ploughing; Polymer; Polymertype; Quantification; Site; Structure; Terrestrial Pollution; Topsoil
    Type: Dataset
    Format: text/tab-separated-values, 2653 data points
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  • 6
    Publication Date: 2023-02-07
    Description: The study took place in Schleswig-Holstein, Northern Germany, in spring 2019. We have chosen 15 arable fields that are part of the federal soil monitoring scheme by LLUR and as such are representative of the different soil conditions in the region. At each of the 15 study fields, boreholes were placed along the corner points of a square of approximately 40 m edge length. At each of the corner points, three boreholes were drilled down to depths of 10, 20 and 30 cm, respectively. As a consequence, we had 4 x 3 x 3 = 36 sampling units with a wet weight of ~ 200 g soil per unit that integrated over soil depths of 0-10 cm, 10-20 cm and 20-30 cm, respectively, per study site. Each sampling unit was dimensioned with a ruler and stored in an individual glass container. Thus, in this study a total of 540 sampling units with a total of 123.3 kg soil material was inspected for plastic particles between 1 and 5 mm. In the laboratory, the wet soil mass of each sampling unit was quantified and then the soil volume was reduced by wet sieving. To facilitate the sieving, the soil was first soaked in lukewarm tap water in a beaker (1 l) to dissolve loamy aggregates. Aggregates that did not dissolve easily were gently broken down with the fingers and carefully homogenized with a metal whisk. Then the soil was placed on a steel analysis sieve with a mesh size of 1 mm and rinsed under running tap water until only particles of 〉 1 mm remained. This material was then transferred into glass petri dishes by using a squeeze bottle made of Polyethylene (PE) filled with tap water and a metal spoon. Excess water was removed from the petri dishes with a disposable syringe (PE and Polypropylene (PP)) and an attached injection cannula (outer diameter 0.8 mm; PP and metal). Next, the content of each petri dish was visually examined twice (once by IK Harms and once by S Troegel) for MP under a stereomicroscope with transmitted light and a 133 Trino Zoom (BMS) with two WF 10x/22 mm oculars. All particles that matched the criteria for the proper identification of MP recommended by Hidalgo-Ruz et al. (2012) were picked and individually placed in 96-well micro test plates that were made from Polystyrene (PS).
    Keywords: DATE/TIME; DEPTH, sediment/rock; Depth comment; Farmland; Identification; Nylon; Ploughing; Polyamide; Polyethylene; Polymer; Polymer, other; Polymer, total; Polymertype; Polymer type; Polypropylene; Quantification; Replicate; Sample mass; Site; Soil water content; Terrestrial Pollution; Topsoil
    Type: Dataset
    Format: text/tab-separated-values, 8654 data points
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  • 7
    Publication Date: 2024-02-07
    Description: Highlights: • Microplastics were found at all of the 15 North German farmland sites sampled. • Mean microplastics' abundance was 3.7 ± 11.9 MP particles per kg DW (median: 0.0, interquartile range: 0.0–4.9). • Composition of microplastics was uniform across the farmland sites sampled. • The most abundant particles were black films made of polyethylene. • Microplastic pollution decreased with soil depths despite regular ploughing. Abstract: The pollution of the aquatic and terrestrial environment with plastics is a fast growing phenomenon with potential threats to the functioning of ecosystems and organisms therein as well as for human well-being. So far, research activities have mainly focused on the occurrence of microplastics (MP) in marine habitats, while little is known about their distribution and composition in the terrestrial environment. Agricultural practices such as fertilization, mulching or ensilage make agriculture a likely path for MP into the environment. Here, we collected soil samples at 15 farmland locations in Schleswig-Holstein, Northern Germany, to study the amount, distribution and composition of MP in the size range between 1 and 5 mm. In total, 379 MP were identified in a total of ~84 kg of dry weight (DW). Particle abundances in the sampling units ranged from 0 to 217.8 MP per kg DW with a mean abundance of 3.7 ± 11.9 MP per kg DW (median: 0.0, interquartile range: 0.0–4.9) per site. Although MP were found at all study sites, only 34% of the sampling units contained synthetic particles. Our data contribute to the establishment of a baseline on the amount, type and size of MP in farmland soils. Such a baseline is important for future monitoring schemes and for the development of more environmentally friendly management systems that reduce the input of MP into the agricultural system.
    Type: Article , PeerReviewed
    Format: text
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