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Crystal structure of [WI2(CO)3{P(OMe)3}2] (1998)

Baker, Paul K. ; Hursthouse, Michael B. ; Latif, Latifah A. ; [et al.]

Springer

Journal of chemical crystallography 28 (1998), S. 639-643

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ISSN: 1572-8854

Keywords: Tungsten(II) ; diiodo ; carbonyl ; trimethylphosphite ; crystal structure

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract [WI2(CO)3{P(OMe)3}2]crystallizes in the orthorhombic space group Pca21, with a = 26.924(5), b = 10.726(2), c = 14.136(3) Å, and Z = 8. There are two molecules in the asymmetric unit, the metal atoms in each case being seven-coordinate with a capped fac-(CO)3 octahedral geometry. The molecular dimensions in the two molecules are nearly identical. The W–P distance to the capping atom 2.397 Å (average) is significantly shorter than the other W–P distance, 2.525 Å (average).

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1023/A:1022469211406

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