Keywords:
Peroxides -- Analysis.
;
Electronic books.
Type of Medium:
Online Resource
Pages:
1 online resource (130 pages)
Edition:
1st ed.
ISBN:
9781483160191
URL:
https://ebookcentral.proquest.com/lib/geomar/detail.action?docID=1822068
Language:
English
Note:
Front Cover -- The Determination of Organic Peroxides -- Copyright Page -- Table of Contents -- PREFACE -- CHAPTER 1. INTRODUCTION -- 1. Lipid Peroxides -- 2 . Polymers -- 3 . Petrochemicals -- 4 . Irradiation -- 5. Miscellaneous -- References -- CHAPTER 2 . STRUCTURE AND REACTIVITY -- 1 . Classification of peroxides -- 2 . Reactivity -- References -- CHAPTER 3. IODOMETRIC METHODS -- 1 . General comments -- 2. Choice of solvent -- 3 . Reaction conditions -- 4 . Titration with thiosulphate -- References -- CHAPTER 4 . FERROUS ION METHODS -- 1 . Introduction -- 2 . Choice of reagent -- 3. Choice of solvent -- 4 . Titration with titanous ions -- 5 . Titration with dichromate ions -- 6 . Titration with mercurous ions -- References -- CHAPTER 5. FURTHER TITRIMETRIC REAGENTS -- 1 . Introduction -- 2 . Arsenious methods -- 3 . Stannous methods -- 4 . Titanous methods -- 5 . Titration with anions -- 6. Sulphides and mercaptans -- References -- CHAPTER 6 . COLORIMETRIC METHODS -- 1 . Introduction -- 2 . Ferrous ions -- 3 . Leuco base of methylene blue -- 4 . Iodine -- 5. iV,A^'-Dimethyl-/?-phenylenediamme -- 6. Other colorimetric reagents -- References -- CHAPTER 7 . POLAROGRAPHIC METHODS -- 1 . Introduction -- 2 . Electrode reaction -- 3 . Polarographic teclmiques for peroxides -- 4 . Nature and concentration of peroxide -- 5 . Solvents and supporting electrolytes -- References -- CHAPTER 8. SPECTROSCOPIC TECHNIQUES -- 1 . Introduction -- 2 . Ultraviolet and visible absorption -- 3 . Infrared absorption -- 4 . Raman spectroscopy -- References -- CHAPTER 9 . CHROMATOGRAPHIC METHODS A. COLUMN CHROMATOGRAPHY -- 1 . Introduction -- 2 . Column techniques -- 3 . Solvent medium -- 4 . Stationary phase -- 5 . Type of peroxide -- References -- CHAPTER 10 . CHROMATOGRAPHIC METHODS B. PAPER CHROMATOGRAPHY -- 1 . Introduction -- 2 . Choice of paper.
,
3. Mobile phase -- 4 . General techniques -- 5 . Chemical structure -- 6 . Detection -- 7 . Class of peroxide -- References -- CHAPTER 11 . CHROMATOGRAPHIC METHODS C. THIN-LAYER CHROMATOGRAPHY -- 1 . Introduction -- 2 . Adsorbents -- 3 . Solvent systems -- 4. Detection -- 5. Techniques -- 6. Applications -- References -- CHAPTER 12. CHROMATOGRAPHIC METHODS D. GAS CHROMATOGRAPHY -- 1. Introduction -- 2. Solid support -- 3. Stationary phase -- 4. Column temperature -- 5. Functional groups -- 6. Quantitative analysis -- References -- CHAPTER 13. CHOICE OF METHOD -- 1. Introduction -- 2. Concentration of peroxide -- 3. Reactivity of peroxide -- 4. Nature of the sample -- INDEX.
