In:
Review of Scientific Instruments, AIP Publishing, Vol. 66, No. 3 ( 1995-03-01), p. 2442-2445
Abstract:
The design and implementation of a pressure cell for the study of hydrothermal reactions by in situ energy dispersive x-ray diffraction is described. The cell permits the study of both the kinetics and mechanism of formation of a wide range of important solid-state compounds such as zeolites and other microporous solids. Reactions can be studied over a wide range of temperature (5–230 °C) and autogenous pressure [0–400 psi (gauge)] conditions. The use of this apparatus is illustrated by a study on the synthesis of a microporous tin chalcogenide phase performed on Station 9.7 of the UK Synchrotron Radiation Source.
Type of Medium:
Online Resource
ISSN:
0034-6748
,
1089-7623
Language:
English
Publisher:
AIP Publishing
Publication Date:
1995
detail.hit.zdb_id:
209865-9
detail.hit.zdb_id:
1472905-2
SSG:
11