Skip to main content
Log in

Experimental Study on Fractal Characteristics of Surface Roughness of Briquettes and their Effect on Wettability of Coal Samples

  • Original Paper
  • Published:
Natural Resources Research Aims and scope Submit manuscript

Abstract

To quantify the influence of surface roughness and its fractal characteristics on the wettability of the samples, coal samples of five particle sizes were selected to produce different cylindrically shaped coal samples in the laboratory, and four grinding methods were used to obtain the coal samples having different roughness values. Three different wetting solutions were utilized to conduct the wetting tests on the coal samples having different roughness values. Theoretical analysis and laboratory studies were carried out to investigate the influence of roughness on wetting parameters. The fractal characteristics of the coal samples with different surface roughness values were analyzed by electron microscopy, and the mechanism of the effect of roughness on wetting performance was analyzed in conjunction with parameters. The results showed that as the surface roughness of the coal samples gradually increased, the fractal dimension increased, the specific surface area of the coal samples increased, the actual contact area of the solid–liquid interface was found to be larger than the apparent contact area, and the adhesion tension and the adhesion work of the wetting solution on the surface of the coal samples increased. The chance of forming a continuous liquid film on the surface of coal samples decreased, more pores were found filled by the wetting solution, resulting in the decrease in contact angle of the liquid on the surface of the coal samples. When the roughness values of the coal samples were in the range of 7–11 μm, the fractal dimension increased rapidly, while the contact angle decreased rapidly.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11
Figure 12
Figure 13
Figure 14
Figure 15
Figure 16
Figure 17

Similar content being viewed by others

References

  • Armstrong, R. T., Sun, C., Mostaghimi, P., Berg, S., Rücker, M., Luckham, P., Georgiadis, A., & McClure, J. E. (2021). Multiscale characterization of wettability in porous media. Transport in Porous Media, 140(1), 215–240.

    Article  Google Scholar 

  • Bingyou, J., Qian, S., & Guanhua, N. (2020). Study on the wettability of a composite solution based on surface structures of coal. ACS Omega, 5(43), 28341–28350.

    Article  Google Scholar 

  • Chakraborty, S., Bisai, R., Palaniappan, S. K., & Pal, S. K. (2022). Characterization of fracture pattern of indian coal measure rock under uniaxial compression stress by statistical analysis of fractal dimension of the microcrack orientation. Journal of The Institution of Engineers (India): Series D, 103(1), 95–106.

    Article  Google Scholar 

  • Chengyong, W., Yaowen, X., Yangchao, X., Rui, Z., Shiwei, W., Kaiyi, S., Jinlong, T., & Xiahui, G. (2020). Investigation of interactions between oxygen-containing groups and water molecules on coal surfaces using density functional theory. Fuel, 287, 119556.

    Google Scholar 

  • Guan, C., Lv, X., Han, Z., & Chen, C. (2020). The wetting characteristics of aluminum droplets on rough surfaces with molecular dynamics simulations. Physical Chemistry Chemical Physics, 22(4), 2361–2371.

    Article  Google Scholar 

  • Han, B., Lu, G.-Y., Zhu, Z.-Q., Guo, Y.-J., & Zhao, Y.-W. (2018). Microstructure features of powdery coal-bearing soil based on the digital image measurement technology and fractal theory. Geotechnical and Geological Engineering, 37(3), 1357–1371.

    Article  Google Scholar 

  • Jia, L., Li, K., Shi, X., Zhao, L., & Linghu, J. (2021). Application of gas wettability alteration to improve methane drainage performance: A case study. International Journal of Mining Science and Technology, 31(04), 621–629.

    Article  Google Scholar 

  • Jiren, T., Jing, Z., Xianfeng, L., Xiangguo, K., Baisheng, N., Dazhao, S., & Tao, Y. (2022). Experimental investigation on the fractal feature of pore-fracture systems in bituminous coal and its influencing factors. Bulletin of Engineering Geology and the Environment, 81(8).

  • Junqing, M., Lijuan, W., Shuo, Z., Yingpei, L., & Junkai, X. (2021). Effect of anionic/nonionic surfactants on the wettability of coal surface. Chemical Physics Letters, 785.

  • Kou, B.-F., & Liu, Q.-Z. (2015). Wetting behavior of hydrophobic dust and dust-fall theory of fine droplets. Brazilian Journal of Physics, 45(6), 708–712.

    Article  Google Scholar 

  • Lei, Q., Xian, Z., Shugang, L., Weikai, W., Siheng, L., & Ping, W. (2022). Fluid space reformation law of liquid nitrogen fracturing coal based on NMR T1–T2 spectra and inspiration for coalbed methane production. Fuel, 324(12), 124811.

    Google Scholar 

  • Lei, Z., Zongqi, L., Dewen, L., Hongtu, W., & Qingtao, Z. (2021). Micromechanism analysis of surfactant wetting of coal based on 13C NMR experiments. ACS Omega, 6(2), 1378–1390.

    Article  Google Scholar 

  • Leilei, S., Nan, D., Jianping, W., Lianchao, S., Lei, W., Zhiwei, L., & Xingming, C. (2022). Gas-liquid competitive adsorption characteristics and coal wetting mechanism under different pre-adsorbed gas conditions. Fuel, 329, 125441.

    Article  Google Scholar 

  • Li, C., Zhang, J., Han, J., & Yao, B. (2021). A numerical solution to the effects of surface roughness on water-coal contact angle. Science and Reports, 11(1), 459.

    Article  Google Scholar 

  • Lianman, X., Hao, W., Xinyue, K., Zhijiao, Q., Jianxin, K., Xinyang, B., & Hui, F. (2022). Study on the change law of physical and mechanical properties and wetting mechanism of coal body under the synergistic effect of chelation-adsorption. Energy Sources, Part A: Recovery, Utilization, and Environmental Effects, 44(2), 4899–4912.

    Google Scholar 

  • Lin, L., Mingpu, L., Jianqiao, L., Xiaoteng, L., Zhihao, L., Mengyu, L., Chuandong, M., Meng, H., Qingbiao, W., Hao, Y., & Xiaofang, Y. (2022b). Effect of bio-based surfactant on wettability of low-rank coal surface and its mechanism. Environmental science and pollution research international, 29(26), 39610–39621.

    Article  Google Scholar 

  • Lin, H., Tian, S., Jiao, A., Cao, Z., Song, K., & Zou, Y. (2022a). Pore characteristics and fractal dimension analysis of tectonic coal and primary-structure coal: A case study of sanjia coal mine in Northern Guizhou. ACS Omega, 7(31), 27300–27311.

    Article  Google Scholar 

  • Liying, S., Shaocheng, G., Deji, J., Shuo, L., & Xi, C. (2022). Wetting mechanism and experimental study of synergistic wetting of bituminous coal with SDS and APG1214. ACS Omega, 7(1), 17593–17599.

    Google Scholar 

  • Meng, J., Yin, F., Li, S., Zhong, R., Sheng, Z., & Nie, B. (2019a). Effect of different concentrations of surfactant on the wettability of coal by molecular dynamics simulation. International Journal of Mining Science and Technology, 29(4), 577–584.

    Article  Google Scholar 

  • Meng, J., Yin, F., Li, S., Zhong, R., Sheng, Z., & Nie, B. (2019b). Effect of different concentrations of surfactant on the wettability of coal by molecular dynamics simulation. International Journal of Mining Science and Technology, 29(04), 577–584.

    Article  Google Scholar 

  • Ni, G., Li, Z., & Xie, H. (2018). The mechanism and relief method of the coal seam water blocking effect (WBE) based on the surfactants. Powder Technology, 323, 60–68.

    Article  Google Scholar 

  • Qun, Z., Botao, Q., Huizhen, L., & Jin, H. (2022). Changes of physical properties of coal dust with crush degrees and their effects on dust control ability of the surfactant solution spray. Environmental Science and Pollution Research International, 29(22), 1–11.

    Google Scholar 

  • Rui, W., Guoqing, L., & Shanshan, L. (2021a). Experimental investigation of the matrix pore size distribution and inner surface fractal dimension of different-structure high rank coals. Journal of Nanoscience and Nanotechnology, 21(1), 529–537.

    Article  Google Scholar 

  • Rui, Z., Shimin, L., & Siyang, Z. (2021b). Characterization of nano-to-micron sized respirable coal dust: Particle surface alteration and the health impact. Journal of Hazardous Materials, 413, 125447.

    Article  Google Scholar 

  • Savitskyi, D. P. (2015). Impact of the pH on angles of contact of water wettability of brown coal. Journal of Water Chemistry and Technology, 37(4), 155–160.

    Article  Google Scholar 

  • Tao, P., Yue, C., Liya, W., Dongmin, M., Guofu, L., Weibo, L., Chao, Z., Yusong, J., Zhuoyuan, M., Peng, H., & Xin, W. (2022). Mechanism of methane adsorption/desorption in low-rank Vitrain and Durain coal affected by pore structure and wettability: a case study in Dafosi Area, South Ordos Basin, China. Energies, 15(14), 5094.

    Article  Google Scholar 

  • Ting, L. Y., Mei, L. H., Zhong, G. M., Qi, Y. S., Yun, Z., Jing, X., Kang, L. G., Jun, L. J., Ming, L. L., Jie, D., & Qi, Z. W. (2021). Experimental and molecular dynamics study into the surfactant effect upon coal wettability. RSC Advances, 11(40), 24543–24555.

    Article  Google Scholar 

  • Wang, X., Yuan, S., & Jiang, B. (2019). Experimental investigation of the wetting ability of surfactants to coals dust based on physical chemistry characteristics of the different coal samples. Advanced Powder Technology, 30(8), 1696–1708.

    Article  Google Scholar 

  • Weiqing, Z., Qiang, H., Shuguang, J., Li, W., Jun, C., & Jingxin, M. (2022). Experimental study on coal dust wettability strengthened by surface active ionic liquids. Environmental Science and Pollution Research International, 29(30), 46325–46340.

    Article  Google Scholar 

  • Xianfeng, L., Xiangguo, K., Baisheng, N., Dazhao, S., Xueqiu, H., & Longkang, W. (2021). Pore Fractal Dimensions of Bituminous Coal Reservoirs in North China and Their Impact on Gas Adsorption Capacity. Natural Resources Research, 30(6).

  • Xiaoming, W., Zheng, D., Shihui, H., Yudong, Y., Xingjin, W., & Sidong, P. (2021). Fractal characteristics of pulverized high volatile bituminous coals with different particle size using gas adsorption. Fuel(prepublish).

  • Xiaonan, W., Shujie, Y., & Bingyou, J. (2019). Wetting process and adsorption mechanism of surfactant solutions on coal dust surface. Journal of Chemistry, 2019.

  • Xiaoxue, L., Liang, W., Jintuo, Z., Peng, C., Qingquan, L., & Tao, Y. (2021). Experimental study on the wettability of tectonic soft coal in Huaibei mining area, China. Energy & Fuels, 35(8).

  • Yingying, H., Qingtao, Z., Gang, Z., Haiyang, W., Yanlong, B., & Yejiao, L. (2021). Influence mechanism of surfactants on wettability of coal with different metamorphic degrees based on infrared spectrum experiments. ACS Omega, 6(34), 22248–22258.

    Article  Google Scholar 

  • Yu, X., Regenauer-Lieb, K., & Tian, F.-B. (2020). Effects of surface roughness and derivation of scaling laws on gas transport in coal using a fractal-based lattice Boltzmann method. Fuel, 259, 116229.

    Article  Google Scholar 

  • Yumeng, Y., Jiangzhong, L., & Mingyi, C. (2022). Superfine comminution characteristics of low-rank coal pyrolysis semicokes and evolution of fragmentation fractal dimension. Fuel, 325, 124991.

    Article  Google Scholar 

  • Zhang, H., Nie, W., Yan, J., Bao, Q., Wang, H., Jin, H., Peng, H., Chen, D., Liu, Z., & Liu, Q. (2020a). Preparation and performance study of a novel polymeric spraying dust suppression agent with enhanced wetting and coagulation properties for coal mine. Powder Technology, 364, 2942.

    Article  Google Scholar 

  • Zhang, Q., Zhou, G., Hu, Y., & Wang, W. (2020b). Experimental investigation on wetting mechanism for coal dust with different metamorphic degree based on infrared spectrum and 13C-NMR. Surface and Interface Analysis, 52(8).

Download references

Acknowledgments

This study is supported by the National Natural Science Foundation of China (No. 52274228, No. 51874236, No. 51674192, No. 51604220).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Min Yan.

Ethics declarations

Conflict of Interest

The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Yan, M., Luo, H., Yang, T. et al. Experimental Study on Fractal Characteristics of Surface Roughness of Briquettes and their Effect on Wettability of Coal Samples. Nat Resour Res 32, 1235–1249 (2023). https://doi.org/10.1007/s11053-023-10174-8

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11053-023-10174-8

Keywords

Navigation