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  • 1
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (273 pages)
    Edition: 1st ed.
    ISBN: 9780080493879
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Front Cover -- NMR Spectroscopy -- Copyright Page -- Contents -- List of Contributors -- Preface -- Chapter 1. In Vivo Proton NMR Studies in Skeletal Musculature -- 1. Introduction -- 2. Structure and function of musculature -- 3. Characteristics of muscle tissue in MR imaging -- 4. Signal patterns in proton spectra of skeletal muscle -- 5. Quantification of spectral signals -- 6. Assessment of relaxation times, MT effects and diffusion characteristics -- 7. Studies on lipid metabolism in skeletal musculature -- 8. Characterization of muscle diseases -- 9. Muscle spectroscopy at higher field strength -- 10. Muscle spectroscopy using other nuclei than protons -- Acknowledgements -- References -- Chapter 2. Quality Assessment of Horticultural Products by NMR -- 1. Introduction -- 2. NMR quality assurance of harvested fruit -- 3. NMR quality assurance of vegetables -- 4. NMR quality assurance of bulbs -- 5. The cellular origins of relaxation and diffusion contrast -- 6. On-line NMR sensor design -- 7. Concluding remarks -- Acknowledgements -- References -- Chapter 3. Applications of NMR to Thermostable Proteins -- 1. Introduction -- 2. Thermostable proteins -- 3. Extremophilic organisms -- 4. Factors determining protein thermostability -- 5. NMR of thermostable proteins -- References -- Chapter 4. High Pressure NMR Studies on Lyotropic Lipid Mesophases and Model Biomembranes -- 1. Introduction -- 2. High-pressure NMR measurements -- 3. Pressure effects on the structure, dynamics and phase transitions of phospholipid vesicles -- 4. Conclusions -- Acknowledgements -- References -- Chapter 5. Diffusion in a Closed Sphere -- 1. Introduction -- 2. The pulsed field gradient echo (PFGE) NMR experiment -- 3. The diffusion equation -- 4. The propagator for one-dimensional diffusion -- 5. Free diffusion -- 6. Diffusion in a box. , 7. Three-dimensional diffusion in a spherically symmetric system -- 8. Conclusion -- References -- Chapter 6. Automatic Analysis of NMR Spectra -- 1. Introduction -- 2. Spectral processing -- 3. Spectral analysis -- 4. Spectral prediction -- 5. Confirmation of structure -- 6. Requirements of multiple parallel synthesis or combinatorial chemistry -- 7. Structural elucidation -- 8. Conclusions -- References -- Index.
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  • 2
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (237 pages)
    Edition: 1st ed.
    ISBN: 9780080551944
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Cover -- Annual reports on NMR spectroscopy -- Copyright -- List of Contributors -- Preface -- Contents -- Flow techniques in NMR spectroscopy -- 1. Introduction -- 2. The Start of Flow NMR and the Evolution of LC-NMR -- 3. Non-Chromatographic Flow NMR -- 4. New Technologies to Facilitate Flow NMR -- 5. Variations of the Flow Techniques/Fluidics -- 6. Applications -- 7. Problems and Challenges -- 8. Conclusions -- Acknowledgments -- References -- Vanadium-51 NMR -- 1. Introduction -- 2. Isotropic Systems -- 3. Solid-State Parameters -- 4. Mesophases -- 5. Computational Methods -- 6. Concluding Remarks -- Acknowledgments -- References -- Solid-State Effects on NMR Chemical Shifts -- 1. Introduction -- 2. Origin of Solid-State Effects on Chemical Shifts -- 3. Theoretical Methods -- 4. Case Studies of Solid-State Effects -- 5. Concluding Remarks -- Acknowledgments -- References -- NMR Studies of Encapsulated Macromolecules -- 1. Introduction -- 2. The Challenge of Complex Biomacromolecules -- 3. The Rate of NMR Relaxation Depends on the Molecular Tumbling Rate -- 4. Reverse Micelles -- 5. Water in Reverse Micelles -- 6. Thermodynamics of Reverse Micelle Particle Formation -- 7. Proteins Encapsulated by Reverse Micelles -- 8. Encapsulation Protocols -- 9. Solvent Suppression -- 10. Hydrodynamic Behavior of AOT Reverse Micelle Assemblies -- 11. Practical Application of Reverse Micelle Encapsulation to Larger Polypeptides -- 12. Multinuclear Resonance Assignments of Encapsulated Proteins -- 13. Structural Studies of Encapsulated Macromolecules -- 14. Low Temperature NMR Studies of Encapsulated Water -- 15. Thermodynamics of Water Shedding - A Concise Analysis -- 16. Low Temperature Studies of Encapsulated Proteins -- 17. Effect of Reverse Micelle Encapsulation on Motional Dynamics in Polypeptides -- 18. Future Studies -- Acknowledgments -- References. , Index.
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  • 3
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (200 pages)
    Edition: 1st ed.
    ISBN: 9780323851046
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Intro -- Annual Reports on NMR spectroscopy -- Copyright -- Contents -- Contributors -- Preface -- Chapter One: Indirect spin-spin coupling constants across noncovalent bonds -- 1. Introduction -- 2. Pnicogen bonded complexes -- 2.1. Indirect spin-spin couplings across PP pnicogen bond -- 2.2. Indirect spin-spin couplings across NP pnicogen bond -- 2.3. Indirect spin-spin couplings across XP pnicogen bond, where X=B, C, O, S, F, and Cl -- 3. Halogen bonded complexes -- 3.1. Indirect spin-spin coupling constants across ClP halogen bond -- 3.2. Indirect spin-spin coupling constants across ClC halogen bond -- 3.3. Indirect spin-spin coupling constants across XN halogen bond, where X=Cl, Br, and I -- 3.4. Indirect spin-spin coupling constants across ClB halogen bond -- 3.5. Indirect spin-spin coupling constants across dihalogen bond -- 4. Tetrel and chalcogen bonded complexes -- 5. Aerogen bonded complexes -- 6. Through-space indirect spin-spin coupling constants -- 7. Conclusions -- References -- Chapter Two: Solid state NMR studies of layered double hydroxides -- 1. Introduction -- 2. Structure and chemical composition of LDH in relation to SSNMR studies -- 2.1. Hydrotalcite LDH M(II)1-xM(III)x(OH)2AnH2O -- 2.2. The structure of LDH derived from aluminium hydroxide -- 3. Acquisition, analysis, and interpretation of SSNMR spectra of LDH-Practical aspects -- 4. Structural characterization of LDH by SSNMR -- 4.1. SSNMR studies of the cation layer -- 4.1.1. Al SSNMR studies of M(II)Al-LDH -- 4.1.2. Li SSNMR studies of LiAl2-LDH -- 4.1.3. Al SSNMR studies of MAl4-LDH -- 4.1.4. Ga SSNMR studies of MgGa-LDH -- 4.1.5. The M(II) ions in hydrotalcite, hydrocalumite and MAl4-LDH -- 4.1.6. O SSNMR studies of LDH -- 4.2. H SSNMR studies of the hydrogen species in LDH -- 4.3. SSNMR studies of anions in the LDH interlayer -- 4.3.1. Carbonate -- 4.3.2. Halides. , 4.3.3. Other oxyanions including nitrate, phosphate, chlorate, and selenate -- 4.3.4. Organic anions -- 5. LDH properties investigated by SSNMR -- 5.1. Drug delivery -- 5.2. Environmental science and remediation -- 6. Conclusions -- Acknowledgements -- References -- Chapter Three: Applications of fast field cycling NMR relaxometry -- 1. Introduction -- 2. The importance of T1 and what does it measure -- 3. The FFC NMR relaxometry NMR experiment in practice -- 4. Understanding soils by FFC NMR relaxometry -- 5. Fast field cycling NMR in the analysis of sediments -- 6. Applications to biochar science -- 7. FFC NMR relaxometry and the dynamics of inorganic salt aqueous solutions -- 8. FFC NMR relaxometry and the dynamics of dissolved organic matter -- 9. Applications in food science -- 9.1. Extra-virgin olive oils -- 9.2. Vinegar and wines -- 9.3. Dairy products -- 9.4. Meat -- 9.5. Honey -- 9.6. Fruits -- 10. Applications in material science -- 10.1. Cement and cement-based systems -- 10.2. Ionic liquids -- 11. Conclusions and perspectives -- References.
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  • 4
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (64 pages)
    Edition: 1st ed.
    ISBN: 9780323988766
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
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  • 5
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (247 pages)
    Edition: 1st ed.
    ISBN: 9780123810427
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Front Cover -- Annual Reports on NMR Spectroscopy -- Copyright Page -- Contents -- Contributors -- Preface -- Chapter 1. Applications of [sup(33)]S NMR Spectroscopy -- 1. Introduction -- 2. NMR Spectroscopic Properties of Sulphur-33 -- 3. [sup(33)]S NMR Parameters -- 4. [sup(33)]S NMR Parameters and Molecular Structure -- 5. Theoretical Calculations of [sup(33)]S NMR Parameters -- References -- Appendix -- Chapter 2. NMR of Peptide Toxins -- 1. Introduction -- 2. NMR as a Tool for Determining the Structures of Toxins -- 3. Microbial Toxins -- 4. Plant Toxins -- 5. Animal Toxins -- 6. Conclusions and Outlook -- Acknowledgements -- References -- Chapter 3. Application of NMR Spectroscopy in Isotope Effects Studies -- 1. Introduction -- 2. Isotope Effects on Chemical Shifts and Spin-Spin Coupling Constants -- 3. Kinetic Isotope Effects Measured at Natural Abundance -- 4. Kinetic Isotope Effect Studies of Reaction Mechanisms by NMR Spectroscopy -- 5. Conclusions -- Acknowledgements -- References -- Chapter 4. Residual Dipolar Couplings for the Configurational and Conformational Analysis of Organic Molecules -- 1. Introduction -- 2. Theory -- 3. Alignment Media for Weak Alignment -- 4. Scaling of Alignment -- 5. Pulse Sequences -- 6. Applications -- 7. Conclusion and Outlook -- Acknowledgements -- References -- Subject Index -- A -- B -- C -- D -- E -- F -- G -- H -- I -- K -- L -- M -- N -- O -- P -- Q -- R -- S -- T -- V -- W -- Color Plates.
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  • 6
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (181 pages)
    Edition: 1st ed.
    ISBN: 9780123973047
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Intro -- Front cover -- Annual Reports on NMR Spectroscopy -- Copyright -- Contents -- Contributors -- Preface -- Chapter 1: Getting the Most Out of HSQC and HMBC Spectra -- 1 Introduction -- 2 HSQC Spectra -- 2.1 HSQC versus HMQC -- 2.2 The performance of modified HSQC sequences -- 2.3 Optimized acquisition and processing parameters for HSQC spectra -- 3 HMBC Spectra -- 3.1 Optimizing acquisition and processing parameters for HMBC spectra -- 3.2 The impact of modifications of HMBC -- 3.3 The advantages and disadvantages of key HMBC variants -- 4 Experimental -- 5 Conclusions -- References -- Chapter 2: A Review of REDCRAFT: Simultaneous Investigation of Structure and Dynamics of Proteins from RDC Restraints -- 1 Introduction -- 2 Residual Dipolar Couplings -- 2.1 Experimental aspects of RDC data acquisition -- 2.2 Theoretical background -- 2.3 Molecular frame, alignment frame and order tensor -- 2.4 Utility of RDCs -- 3 A Comparison of RDCs to NOEs -- 3.1 Sensitivity of protein structure determination from RDCs versus NOEs -- 3.2 Summary of advantages in structure determination of proteins from RDCs -- 4 Existing Software for Structure Determination from RDC Data -- 5 Redcraft -- 5.1 REDCRAFT algorithm -- 5.2 Software engineering aspects -- 5.3 Practical aspects of REDCRAFT -- 5.3.1 Input -- 5.3.2 Downloading, installation, and compilation -- 5.3.3 Integration of REDCRAFT with other software packages -- 6 Structure Determination with REDCRAFT -- 6.1 Structure determination from six RDCs per residue in two alignment media -- 6.2 Structure determination from four RDCs per residue in two alignment media -- 6.3 Structure determination from three RDCs per residue in two alignment media -- 6.4 Structure determination from N-H and Cα-Hα RDCs in two alignment media -- 7 Simultaneous Study of Structure and Dynamics. , 7.1 Dynamic profile analysis of REDCRAFT -- 7.2 Fragmented study of rigid body dynamics -- 8 Conclusion -- Acknowledgements -- References -- Chapter 3: NMR Studies of Solid-State Dynamics -- 1 Introduction -- 2 NMR Relaxation and Relaxometry -- 2.1 Principles of field-dependent relaxometry -- 2.2 Relaxation times and correlation functions -- 2.3 Field-dependent relaxation in simple crystal lattices -- 2.4 Relaxometry and translational diffusion -- 2.5 Validity ranges of classical relaxation theories -- 2.6 Relaxation processes and quadrupolar interactions -- 2.6.1 Cross-relaxation -- 2.6.2 Polarization transfer effects -- 2.6.3 Quadrupolar relaxation enhancement -- 2.7 Single-frequency relaxation studies -- 2.8 Relaxation processes and slow dynamics -- 2.9 Relaxation dispersion and motional models -- 3 Nuclear Quadrupolar Resonance Spectroscopy -- 3.1 NQR spectra between and motional models -- 4 Analogy between NQR and ESR -- 5 Concluding Remarks -- Acknowledgements -- References -- Chapter 4: Earth's Field Spectroscopy -- 1 Introduction -- 2 Experimental Techniques -- 2.1 Sensitivity enhancements -- 2.2 Environmental concerns -- 3 Observable Phenomena -- 3.1 Chemical shift -- 3.2 Homo- and heteronuclear J couplings -- 4 Calculation of Spectra -- 5 Path from Weak to Strong Coupling -- 6 Conclusion -- References -- Subject Index.
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  • 7
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Spectrum analysis. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (288 pages)
    Edition: 1st ed.
    ISBN: 9780080461977
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Cover -- Annual reports on NMR Spectrocopy -- Copyright -- List of Contributors -- Preface -- Contents -- Applications of 29Si NMR Parameters -- 1. Introduction -- 2. Experimental -- 3. Nuclear Spin Relaxation -- 4. Chemical Shifts δ29Si -- 5. Indirect Nuclear Spin-Spin Coupling Constants nJ(29Si,X) -- 6. Conclusions -- References -- NMR Studies of b-Type Haemoproteins Reconstituted with a Ring-Fluorinated Haem -- 1. Introduction -- 2. Haemoprotein -- 3. 19F Labeling of b-Type Haemoprotein Using Reconstitution -- 4. Effect of 19F Labeling on the Electronic Structure of Porphyrin -- 5. NMR Spectral Comparison of Haem bis-CYANO Complexes -- 6. Properties of Myoglobins Reconstituted with Fluorinated Haems -- 7. 19F NMR Spectral Properties of Myoglobins Reconstituted with Fluorinated Haems -- 8. 19F NMR Studies of Myoglobins Reconstituted with Fluorinated Haems -- 9. Concluding Remarks -- References -- Site-Directed Solid-State NMR on Membrane Proteins -- 1. Introduction -- 2. Isotope Enrichment -- 3. Site-Directed Assignment of 13C NMR Peaks of Membrane Proteins -- 4. Backbone Dynamics and Structures in the Interfacial Domains of Bacteriorhodopsin from Purple Membrane -- 5. Backbone Dynamics in the Transmembrane α-Helices -- 6. Backbone Structures and Dynamics in Monomers -- 7. Membrane Proteins Overexpressed in E. coli -- 8. Membrane-Binding Protein -- 9. Concluding Remarks -- Acknowledgements -- References -- High-Pressure NMR Studies in Proteins -- 1. Introduction -- 2. High-Pressure NMR spectroscopy -- 3. Application of high-pressure NMR spectroscopy on proteins -- 4. Conclusions -- Acknowledgments -- References -- Xenon NMR Spectroscopy -- 1. Introduction -- 2. Conventional Xenon NMR Studies -- 3. Hyperpolarized Xenon -- 4. Conclusion -- Acknowledgments -- References -- Index.
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  • 8
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Nuclear spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (369 pages)
    Edition: 1st ed.
    ISBN: 9780080584003
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Front Cover -- Annual Reports on NMR Spectroscopy, Volume 17 -- Copyright Page -- Contents -- List of Contributors -- Preface -- Chapter 1. Theoretical Aspects of Isotope Effects on Nuclear Shielding -- I. Introduction -- II. Rovibrational effects on nuclear shielding -- III. Isotope shifts in diatomic molecules -- IV. One-bond isotope shifts in polyatomic molecules -- V. Isotope effects over more than one bond -- VI. Temperature and solvent effects on isotope shifts -- VII. Conclusions -- Acknowledgment -- References -- Chapter 2. NMR Spectroscopy of Paramagnetic Haem Proteins -- I. Introduction -- II. Assignment methods -- III. Selected problems of biological relevance -- IV. Other nuclei -- Acknowledgments -- References -- Chapter 3. Nuclear Magnetic Relaxation and Models for Backbone Motions of Macromolecules in Solution -- I. Introduction -- II. Experimental methods -- III. Theory -- IV. Correlation functions for polymer motions -- V. Conclusions -- References -- Chapter 4. Nuclear Magnetic Resonance of Less Common Quadrupolar Nuclei -- I. Introduction -- II. Alkali metals (except Li and Na) -- III. Alkaline earth nuclei -- IV. Main groups III and IV -- V. Main groups V and VI -- VI. Transition elements -- VII. Conclusions -- Acknowledgment -- References -- Chapter 5. Platinum NMR Spectroscopy -- I. Introduction -- II. Methodology -- III. Referencing -- IV. Chemical shifts -- V. Couplings -- VI. Applications -- VII. Tables -- References -- Index.
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  • 9
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Nuclear spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (261 pages)
    Edition: 1st ed.
    ISBN: 9780080584164
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Front Cover -- Annual Reports on NMR Spectroscopy, Volume 33 -- Copyright Page -- Contents -- List of Contributors -- Preface -- Chapter 1. Applications of Field-Cyding NMR -- 1. Introduction -- 2. Basic field-cycling concepts -- 3. Applications -- 4. Other developments and outlook -- Acknowledgements -- References -- Chapter 2. Progress in High Resolution NMR in Solids -- 1. Introduction -- 2. Interactions -- 3. Polarization transfer and irreversible processes -- 4. Suppression of interactions -- 5. Recovery of interactions -- 6. Multi-quantum coherence -- 7. Zero field -- Acknowledgements -- References -- Chapter 3. High Pressure NMR -- 1. Introduction -- 2. NMR instrumentation for high-pressure work -- 3. High-pressure NMR studies of model membranes -- 4. Applications of two-dimensional techniques at high pressure -- 5. Survey of recent high-pressure NMR studies -- Acknowledgements -- References -- Chapter 4. Molybdenum-95 NMR Spectroscopy -- 1. Molybdenum-95 NMR -- 2. Solution state NMR -- 3. Chromium and tungsten NMR -- 4. Solid-state NMR -- 5. Concluding remarks -- References -- Appendix -- Chapter 5. Applications of Solid-state NMR in Oil Shale Research -- 1. Introduction -- 2. 13C NMR in solids -- 3. Quantification -- 4. Applications of 13C NMR -- 5. Applications of 1H NMR -- Concluding remarks -- References -- Index.
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  • 10
    Online Resource
    Online Resource
    San Diego :Elsevier Science & Technology,
    Keywords: Nuclear magnetic resonance spectroscopy. ; Nuclear spectroscopy. ; Electronic books.
    Type of Medium: Online Resource
    Pages: 1 online resource (499 pages)
    Edition: 1st ed.
    ISBN: 9780080584133
    Series Statement: Issn Series
    DDC: 543.0877
    Language: English
    Note: Front Cover -- Annual Reports on NMR Spectroscopy, Volume 30 -- Copyright Page -- Contents -- List of Contributors -- Preface -- Chapter 1. Calculation and Prediction of Structural NMR Shifts in Respiratory Proteins -- 1. Introduction -- 2. Theoretical Approach to NMR Parameters -- 3. Shielding Dependence on Protein Structure -- 4. Long-range Effects on NMR Parameters -- 5. Property Correlations in Respiratory Proteins -- Acknowledgement -- References -- Chapter 2. NMR Applications to Porous Solids -- 1. Introduction -- 2. NMR studies of microporous materials -- 3. NMR studies of mesoporous materials -- 4. 129Xe NMR studies of porous materials -- 5. NMR studies of molecular transport in porous solids -- Acknowledgement -- References -- Chapter 3. Miscibility, Morphology and Molecular Motion in Polymer Blends -- 1. Introduction -- 2. Miscibility -- 3. Polymer-polymer interaction -- 4. Morphology -- 5. Molecular motion -- Note added in proof -- Acknowledgement -- References -- Chapter 4. One-bond 13C-13C Spin-Spin Coupling Constants -- 1. Introduction -- 2. Theoretical considerations -- 3. Unsubstituted hydrocarbons -- 4. Substituent effects on one-bond CC spin-spin couplings across single, double and triple bonds -- 5. One-bond CC spin-spin coupling constants in derivatives of benzene -- 6. One-bond CC coupling constants in heteroaromatic systems -- 7. One-bond CC couplings in substituted aliphatic cyclic and heterocyclic systems -- 8. The lone pair effect -- 9. One-bond CC couplings in structural studies of complexes -- 10. One-bond CC couplings in charged molecules and some related compounds -- 11. One-bond CC couplings in biological studies -- 12. Experimental methods -- 13. Application of the INADEQUATE method in structural elucidations -- Note added in proof -- References -- Chapter 5. Carbon-13 NMR Spectra of Sesquiterpene Lactones. , 1. Introduction -- 2. Structure classification -- 3. Methods of structure determination -- 4. Carbon-13 NMR spectra -- References -- Index -- Cumulative Indexes for Authors and Subjects, Volumes 21-30.
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