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  • 1
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 85 (2002), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Using monolithic alumina ceramics as the reference, the thermal shock behavior of the hot-pressed alumina matrix ceramics with 3 mol% neodymium titanate was investigated. The thermal shock resistance of the materials was evaluated by water quenching and a subsequent three-point bending test to determine the flexural strength degradation. The hot-pressed composite exhibited a temperature differential of the thermal shock resistance 120°C higher than the monolith, mainly because of significantly improved fracture toughness.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The compaction behavior of fine alumina powders with different particle sizes or bimodal particle-size distributions that are undergoing pressure filtration was investigated. Three alumina powders—average particle sizes of 0.2—0.86 μm—were compacted to a solids fraction of 62—65 vol% from suspensions at pH 3, which was the pH level at which the suspensions showed their lowest viscosity. When the powders of different average sizes were mixed, the suspensions showed better flowability, and the lowest viscosity was obtained when the fraction of fines was ∼30 vol% and pH = 3. The mixed-sized powder suspensions were compacted to higher density than the suspensions of unmixed fine or coarse powders, and the maximum density was obtained for mixed suspensions that had the lowest viscosity, despite the different particle-size ratio. Maximum densities of 72.5% and 75.0% were attained when the size ratios were 2 and 5, respectively. The compacts that were pressure-filtered from mixed suspensions exhibited a single-peaked pore-size distribution and a homogeneous microstructure, whereas the pore-size distributions of dry-pressed compacts were double-peaked. The sintering behavior of the compacts that were pressure-filtrated from bimodal powders exhibited significantly better sinterability and much-less linear shrinkage than the coarser powders and the dry-pressed powder compacts.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 82 (1999), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Flexure creep and creep-recovery behavior were investigated for monolithic Al2O3 and 10-vol%-SiC-particle-reinforced Al2O3-matrix composites in an air atmosphere at temperatures of 1160°-1400°C. Two types of SiC particles were used: one has an average size of 2.7 µm and has an amount of SiO2 impurities per unit surface area that is one order of magnitude higher than the other, which has an average size of 0.6 µm. Compared to the creep behavior of monolithic Al2O3, the strain rate of the composites with the 0.6 µm SiC particles (denoted here as S-10) did not decrease; the composites with the 2.7 µm SiC particles (denoted here as L-10) exhibited excellent creep resistance. This difference was related to the microstructural features and the oxidation behavior of the composites: the Al2O3 grains in S-10 were mainly equiaxed, only ∼10% of the Al2O3 grains were elongated, and most of the SiC particles that resided at the grain boundaries or at triple-grain junctions were oxidized during creep, whereas the Al2O3 grains in L-10 were mostly irregularly shaped and elongated and most of the SiC particles were entrapped in the Al2O3 matrix grains, which prevented the oxidation of the SiC particles. These different microstructural features were associated with different amounts of SiO2 impurity content per unit surface area on the SiC particle surfaces. In addition, the monolithic Al2O3 showed no anelastic recovery when the load was removed; however, the composites exhibited significant anelastic recovery, especially for L-10. This phenomenon was attributed to the elongated grain morphology.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 121-123 (Mar. 2007), p. 69-73 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: High ordered mesoporous carbon molecular sieves designated as CMK-3 and CMK-5was synthesized using mesoporous silica SBA-15 as hard template, pre-polymerized furfurylalcohol as a carbon souse by one-step impregnation. The effect of the furfuryl alcohol to silicasratio have been investigated. XRD pattern, N2 sorption, FE-SEM, TEM, TG-DSC was used tocharacterize the property of the product. These results show that the CMK-3 and CMK-5 typemesoporous carbon can be controlled and facilely obtained
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 121-123 (Mar. 2007), p. 473-478 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: A family of mesoporous multilamellar silica vesicles has been successfully synthesizedby using P123 as structure directing agent and hexane as co-surfactant. The structure wascharacterized with XRD, TEM, and N2 adsorption-desorption isotherms. This multilamellar silicavesicle materials process high specific area, large pore volume, and a bimodale pore sizedistribution. Furthermore, these materials are stable when the surfactant is removed at 530 oC
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 121-123 (Mar. 2007), p. 5-8 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: A novel and thermally stable hierarchically porous yttrium doped zirconiamaterial with crystallized framework has been synthesized in a facile process. XRD,nitrogen adsorption analysis, FESEM, FETEM, were used for the structuralcharacterizations. This novel hierarchically porous zirconia shows a well-definedordered macroporous structure, a broad distributed mesoviods, and a very uniformmesoporous pore-distribution. Small amount of yttrium can be helpful to increase thethermal stability of the prepared hierarchically porous zirconium oxide
    Type of Medium: Electronic Resource
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