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  • 1
    Publication Date: 2023-06-17
    Description: Knowledge of pressure-dependent static and dynamic moduli of porous reservoir rocks is of key importance for evaluating geological setting of a reservoir in geo-energy applications. We examined experimentally the evolution of static and dynamic bulk moduli for porous Bentheim sandstone with increasing confining pressure up to about 190 MPa under dry and water-saturated conditions. The static bulk moduli (Ks) were estimated from stress–volumetric strain curves while dynamic bulk moduli (Kd) were derived from the changes in ultrasonic P- and S- wave velocities (~ 1 MHz) along different traces, which were monitored simultaneously during the entire deformation. In conjunction with published data of other porous sandstones (Berea, Navajo and Weber sandstones), our results reveal that the ratio between dynamic and static bulk moduli (Kd/Ks) reduces rapidly from about 1.5 − 2.0 at ambient pressure to about 1.1 at high pressure under dry conditions and from about 2.0 − 4.0 to about 1.5 under water-saturated conditions, respectively. We interpret such a pressure-dependent reduction by closure of narrow (compliant) cracks, highlighting that Kd/Ks is positively correlated with the amount of narrow cracks. Above the crack closure pressure, where equant (stiff) pores dominate the void space, Kd/Ks is almost constant. The enhanced difference between dynamic and static bulk moduli under water saturation compared to dry conditions is possibly caused by high pore pressure that is locally maintained if measured using high-frequency ultrasonic wave velocities. In our experiments, the pressure dependence of dynamic bulk modulus of water-saturated Bentheim sandstone at effective pressures above 5 MPa can be roughly predicted by both the effective medium theory (Mori–Tanaka scheme) and the squirt-flow model. Static bulk moduli are found to be more sensitive to narrow cracks than dynamic bulk moduli for porous sandstones under dry and water-saturated conditions.
    Description: Helmholtz-Zentrum Potsdam Deutsches GeoForschungsZentrum - GFZ (4217)
    Keywords: ddc:550.78 ; Porous sandstone ; Static bulk modulus ; Dynamic bulk modulus ; Narrow (compliant) cracks ; Equant (stiff) pores
    Language: English
    Type: doc-type:article
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  • 2
    Publication Date: 2023-11-15
    Description: This is a repond to the comments raised in Crisci´s et al. paper “Discussion on “Experimental Deformation of Opalinus Clay at Elevated Temperature and Pressure Conditions ¬ Mechanical Properties and the Influence of Rock Fabric” (2021). We are pleased to use the opportunity to clarify issues related to testing procedures and interpretation in more detail.
    Description: Bundesministerium für Bildung und Forschung http://dx.doi.org/10.13039/501100002347
    Description: Helmholtz-Gemeinschaft http://dx.doi.org/10.13039/501100001656
    Description: Helmholtz-Zentrum Potsdam Deutsches GeoForschungsZentrum - GFZ (4217)
    Keywords: ddc:550.78 ; Opalinus Clay ; Testing procedure ; Pore pressure generation ; Strain rate ; Drying-induced micro cracks
    Language: English
    Type: doc-type:article
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  • 3
    Publication Date: 2023-11-15
    Description: The mechanical behavior of the sandy facies of Opalinus Clay (OPA) was investigated in 42 triaxial tests performed on dry samples at unconsolidated, undrained conditions at confining pressures (pc) of 50–100 MPa, temperatures (T) between 25 and 200 °C and strain rates (ε˙) of 1 × 10〈sup〉–3〈/sup〉–5 × 10〈sup〉–6〈/sup〉 s〈sup〉−1〈/sup〉. Using a Paterson-type deformation apparatus, samples oriented at 0°, 45° and 90° to bedding were deformed up to about 15% axial strain. Additionally, the influence of water content, drainage condition and pre-consolidation was investigated at fixed p〈sub〉c〈/sub〉–T conditions, using dry and re-saturated samples. Deformed samples display brittle to semi-brittle deformation behavior, characterized by cataclastic flow in quartz-rich sandy layers and granular flow in phyllosilicate-rich layers. Samples loaded parallel to bedding are less compliant compared to the other loading directions. With the exception of samples deformed 45° and 90° to bedding at p〈sub〉c〈/sub〉 = 100 MPa, strain is localized in discrete shear zones. Compressive strength (σ〈sub〉max〈/sub〉) increases with increasing p〈sub〉c〈/sub〉, resulting in an internal friction coefficient of ≈ 0.31 for samples deformed at 45° and 90° to bedding, and ≈ 0.44 for samples deformed parallel to bedding. In contrast, pre-consolidation, drainage condition, T and ε˙ do not significantly affect deformation behavior of dried samples. However, σ〈sub〉max〈/sub〉 and Young’s modulus (E) decrease substantially with increasing water saturation. Compared to the clay-rich shaly facies of OPA, sandy facies specimens display higher strength σmax and Young’s modulus E at similar deformation conditions. Strength and Young’s modulus of samples deformed 90° and 45° to bedding are close to the iso-stress Reuss bound, suggesting a strong influence of weak clay-rich layers on the deformation behavior.
    Description: Bundesministerium für Bildung und Forschung http://dx.doi.org/10.13039/501100002347
    Description: Helmholtz-Gemeinschaft http://dx.doi.org/10.13039/501100001656
    Description: Helmholtz-Zentrum Potsdam Deutsches GeoForschungsZentrum - GFZ (4217)
    Keywords: ddc:550.78 ; Clay rock ; Sandy facies of Opalinus Clay ; Triaxial deformation experiments ; Microstructural deformation mechanisms ; Pressure-, temperature- and strain rate-dependent mechanical behaviour ; Anisotropy
    Language: English
    Type: doc-type:article
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  • 4
    Publication Date: 2024-01-15
    Description: 〈title xmlns:mml="http://www.w3.org/1998/Math/MathML"〉Abstract〈/title〉〈p xmlns:mml="http://www.w3.org/1998/Math/MathML" xml:lang="en"〉Transient creep of crustal rocks is important to explain time‐dependent geological processes such as postseismic deformation following a large continental earthquake. While the steady‐state creep flow law parameters of quartz and feldspar, major minerals in the upper and lower crust, are well known, the physical mechanism behind transient creep and the corresponding flow law parameters are poorly understood. We quantify the flow law parameters for both quartz and granulite (mixture of plagioclase and pyroxene) under wet conditions with a nonlinear Burgers model using a Markov chain Monte Carlo (MCMC) method. Modeling results yield an activation energy of 70 ± 20 kJ/mol and a stress exponent of 2.0 ± 0.1 for transient creep of quartz aggregates. For granulite/feldspar, we find activation energies of 280 ± 30 and 220 ± 20 kJ/mol and stress exponents of 1.0 ± 0.2 and 0.9 ± 0.1 under mid (1050–1100°C) and high (1125–1150°C), temperature conditions, respectively. The stress exponents and activation energies of transient creep are consistently smaller than those of steady‐state creep for both quartz and granulite/feldspar. Combined with results for transient creep of olivine that were previously obtained (Masuti & Barbot, 2021, 〈ext-link ext-link-type="uri" xlink:href="https://doi.org/10.1186/s40623-021-01543-9"〉https://doi.org/10.1186/s40623-021-01543-9〈/ext-link〉), we suggest that the activation energies and stress exponents of transient creep are smaller than those of steady‐state creep for volumetrically important silicate minerals of the crust and upper mantle. Extrapolation of the estimated flow law parameters of granulite/feldspar to natural conditions suggests that transient creep may dominate during the postseismic period and lasts longer than previously thought.〈/p〉
    Description: Plain Language Summary: Earthquakes induce intermittent deformation of the solid Earth at rates that are higher or lower than the interseismic strain rates. When an earthquake occurs, it is accompanied by a sudden slip on the fault and a rapid stress change in the lower crust leading to an evolving rock strength. Lower crustal rocks represent a complex assembly of minerals and several different micro‐mechanisms may be activated during deformation. We use experimental data for quartz and feldspar to constrain the mechanical properties of the transient creep (i.e., stress changes with strain under constant strain rate conditions or strain changes nonlinearly with time under constant stress conditions). Based on our results, we conclude that the transient creep following an earthquake may not be as short lived as previously has been thought.〈/p〉
    Description: Key Points: 〈list-item〉 〈p xml:lang="en"〉Transient creep flow law parameters of quartz and granulite are determined using a Markov chain Monte Carlo method〈/p〉〈/list-item〉 〈list-item〉 〈p xml:lang="en"〉Low stress exponent of the transient creep in silicates could be due to weak dependency of dislocation density on the stress〈/p〉〈/list-item〉 〈list-item〉 〈p xml:lang="en"〉Transient creep could be dominant during the postseismic phase of the earthquake cycle〈/p〉〈/list-item〉 〈/list〉 〈/p〉
    Description: Japan Society for the Promotion of Science http://dx.doi.org/10.13039/501100001691
    Description: Humboldt Research Fellowship for Postdoctoral Researchers
    Description: Alexander von Humboldt‐Stiftung http://dx.doi.org/10.13039/100005156
    Description: https://doi.org/10.5281/zenodo.8304793
    Description: https://doi.org/10.5281/zenodo.8304760
    Keywords: ddc:550.724 ; transient creep ; quartz ; feldspar ; rheology ; lower crust ; granulite
    Language: English
    Type: doc-type:article
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  • 5
    Publication Date: 2011-06-01
    Description: A series of hematite samples (〉98 % Fe2O3, Sishen Mine, South Africa) with different initial grain sizes of 3) fit to a power law creep equation with a pre-exponential constant of lnA = -5.03 {+/-} 0.61 MPa-2.5 s-1, an activation energy of Q = 249 {+/-} 48 kJ mol-1, and a stress exponent of n = 2.5 {+/-} 0.5, indicating dislocation creep partially assisted by grain boundary sliding as the main deformation mechanism. Irrespective of the initial grain size, the final grain size (D) of fully recrystallized samples decreases continuously with increasing (steady state) equivalent stress ({sigma}), yielding a piezometric relationship of the form: D = 1055 x {sigma} 1.03 {+/-} 0.10. The piezometer is applied to itabiritic hematite ores of the Iron Quadrangle, Minas Gerais, Brazil, consisting mainly of layered hematite and quartz. Compared to hematite the measured recrystallized grain size of quartz is always larger, which is in agreement with the grain size range predicted by recrystallized grain size-based piezometers for hematite and quartz if deformed at similar stress below about 100 MPa.
    Print ISSN: 0935-1221
    Electronic ISSN: 1617-4011
    Topics: Geosciences
    Published by Schweizerbart
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  • 6
    Publication Date: 2021-07-04
    Description: Understanding the relation between injection‐induced seismic moment release and operational parameters is crucial for early identification of possible seismic hazards associated with fluid‐injection projects. We conducted laboratory fluid‐injection experiments on permeable sandstone samples containing a critically stressed fault at different fluid pressurization rates. The observed fluid‐induced fault deformation is dominantly aseismic. Fluid‐induced stick‐slip and fault creep reveal that total seismic moment release of acoustic emission (AE) events is related to total injected volume, independent of respective fault slip behavior. Seismic moment release rate of AE scales with measured fault slip velocity. For injection‐induced fault slip in a homogeneous pressurized region, released moment shows a linear scaling with injected volume for stable slip (steady slip and fault creep), while we find a cubic relation for dynamic slip. Our results highlight that monitoring evolution of seismic moment release with injected volume in some cases may assist in discriminating between stable slip and unstable runaway ruptures.
    Description: Plain Language Summary: Anthropogenic earthquakes caused by fluid injection have been reported worldwide to occur in the frame of waste‐water disposal, CO2 sequestration, and stimulation of hydrocarbon or deep geothermal reservoirs. To study the dynamics of injection‐induced seismic energy release in a controlled environment, we performed laboratory fluid injection experiments on critically stressed high‐permeability sandstone samples with a prefabricated fault. We monitored acoustic emission occurring during injection‐induced fault sliding. We find that the total seismic deformation (expressed as total seismic moment) is related to total injected volume, independent of fault slip modes (i.e., dynamic slip, steady slip, and fault creep). Seismic moment release rate roughly scales with fault slip velocity. In our experiments, the fluid pressure front migrates faster than the rupture front by about 5 orders of magnitude, resulting in fault slip within a zone of homogeneous fluid overpressure. We find that cumulative seismic moment scales linearly with the injected volume for stable slip (steady slip and fault creep), while it follows a cubic relation for dynamic slip. Our experimental results suggest that the deviation of cumulative moment release with injected volume from a linear trend in practice might be a sign for potential seismic risk. This may be considered in modifying current injection strategies.
    Description: Key Points: Injection‐induced fault deformation is dominantly aseismic. Total moment release depends on total injected volume, independent of fault slip behavior. Moment‐injected volume scaling is linear for stable slip but shows a cubic relation for dynamic slip.
    Keywords: 551.22 ; induced seismicity ; seismic moment release ; fluid injection ; stick slip ; fault creep ; acoustic emission
    Type: article
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  • 7
    Publication Date: 2021-10-06
    Description: Understanding the physical mechanisms governing fluid-induced fault slip is important for improved mitigation of seismic risks associated with large-scale fluid injection. We conducted fluid-induced fault slip experiments in the laboratory on critically stressed saw-cut sandstone samples with high permeability using different fluid pressurization rates. Our experimental results demonstrate that fault slip behavior is governed by fluid pressurization rate rather than injection pressure. Slow stick-slip episodes (peak slip velocity 〈 4 μm/s) are induced by fast fluid injection rate, whereas fault creep with slip velocity 〈 0.4 μm/s mainly occurs in response to slow fluid injection rate. Fluid-induced fault slip may remain mechanically stable for loading stiffness larger than fault stiffness. Independent of fault slip mode, we observed dynamic frictional weakening of the artificial fault at elevated pore pressure. Our observations highlight that varying fluid injection rates may assist in reducing potential seismic hazards of field-scale fluid injection projects.
    Keywords: 550.724 ; fault slip ; fluid injection ; induced seismicity ; fluid pressurization rate ; stick-slip ; fault creep
    Language: English
    Type: map
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