GLORIA

GEOMAR Library Ocean Research Information Access

Your email was sent successfully. Check your inbox.

An error occurred while sending the email. Please try again.

Proceed reservation?

Export
  • 1
    Online Resource
    Online Resource
    Elsevier BV ; 2023
    In:  International Journal of Rock Mechanics and Mining Sciences Vol. 171 ( 2023-11), p. 105588-
    In: International Journal of Rock Mechanics and Mining Sciences, Elsevier BV, Vol. 171 ( 2023-11), p. 105588-
    Type of Medium: Online Resource
    ISSN: 1365-1609
    Language: English
    Publisher: Elsevier BV
    Publication Date: 2023
    detail.hit.zdb_id: 2016557-2
    SSG: 19,1
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 2
    In: Solid Earth, Copernicus GmbH, Vol. 12, No. 9 ( 2021-09-23), p. 2109-2126
    Abstract: Abstract. A microphysics-based understanding of mechanical and hydraulic processes in clay shales is required for developing advanced constitutive models, which can be extrapolated to long-term deformation. Although many geomechanical tests have been performed to characterise the bulk mechanical, hydro-mechanical, and failure behaviour of Opalinus Clay, important questions remain about micromechanisms: how do microstructural evolution and deformation mechanisms control the complex rheology? What is the in situ microstructural shear evolution, and can it be mimicked in the laboratory? In this contribution, scanning electron microscopy (SEM) was used to image microstructures in an Opalinus Clay sample deformed in an unconsolidated–undrained triaxial compression test at 4 MPa confining stress followed by argon broad ion beam (BIB) polishing. Axial load was applied (sub-)perpendicular to bedding until the sample failed. The test was terminated at an axial strain of 1.35 %. Volumetric strain measurements showed bulk compaction throughout the compression test. Observations on the centimetre to micrometre scale showed that the samples exhibited shear failure and that deformation localised by forming a network of micrometre-wide fractures, which are oriented with angles of 50∘ with respect to horizontal. In BIB–SEM at the grain scale, macroscale fractures are shown to be incipient shear bands, which show dilatant intergranular and intragranular microfracturing, granular flow, bending of phyllosilicate grains, and pore collapse in fossils. Outside these zones, no deformation microstructures were observed, indicating only localised permanent deformation. Thus, micromechanisms of deformation appear to be controlled by both brittle and ductile processes along preferred deformation bands. Anastomosing networks of fractures develop into the main deformation bands with widths up to tens of micrometres along which the sample fails. Microstructural observations and the stress–strain behaviour were integrated into a deformation model with three different stages of damage accumulation representative for the deformation of the compressed Opalinus Clay sample. Results on the microscale explain how the sample locally dilates, while bulk measurement shows compaction, with an inferred major effect on permeability by an increase in hydraulic conductivity within the deformation band. Comparison with the microstructure of highly strained Opalinus Clay in fault zones shows partial similarity and suggests that during long-term deformation additional solution–precipitation processes operate.
    Type of Medium: Online Resource
    ISSN: 1869-9529
    Language: English
    Publisher: Copernicus GmbH
    Publication Date: 2021
    detail.hit.zdb_id: 2545676-3
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 3
    Online Resource
    Online Resource
    Oxford University Press (OUP) ; 2020
    In:  Geophysical Journal International Vol. 224, No. 3 ( 2020-12-09), p. 1523-1539
    In: Geophysical Journal International, Oxford University Press (OUP), Vol. 224, No. 3 ( 2020-12-09), p. 1523-1539
    Abstract: A comprehensive characterization of clay shale behavior requires quantifying both geomechanical and hydromechanical characteristics. This paper presents a comparative laboratory study of different methods to determine the water permeability of saturated Opalinus Clay: (i) pore pressure oscillation, (ii) pressure pulse decay and (iii) pore pressure equilibration. Based on a comprehensive data set obtained on one sample under well-defined temperature and isostatic effective stress conditions, we discuss the sensitivity of permeability and storativity on the experimental boundary conditions (oscillation frequency, pore pressure amplitudes and effective stress). The results show that permeability coefficients obtained by all three methods differ less than 15 per cent at a constant effective stress of 24 MPa (kmean = 6.6E-21 to 7.5E-21 m2). The pore pressure transmission technique tends towards lower permeability coefficients, whereas the pulse decay and pressure oscillation techniques result in slightly higher values. The discrepancies are considered minor and experimental times of the techniques are similar in the range of 1–2 d for this sample. We found that permeability coefficients determined by the pore pressure oscillation technique increase with higher frequencies, that is oscillation periods shorter than 2 hr. No dependence is found for the applied pressure amplitudes (5, 10 and 25 per cent of the mean pore pressure). By means of experimental handling and data density, the pore pressure oscillation technique appears to be the most efficient. Data can be recorded continuously over a user-defined period of time and yield information on both, permeability and storativity. Furthermore, effective stress conditions can be held constant during the test and pressure equilibration prior to testing is not necessary. Electron microscopic imaging of ion-beam polished surfaces before and after testing suggests that testing at effective stresses higher than in situ did not lead to pore significant collapse or other irreversible damage in the samples. The study also shows that unloading during the experiment did not result in a permeability increase, which is associated to the persistent closure of microcracks at effective stresses between 24 and 6 MPa.
    Type of Medium: Online Resource
    ISSN: 0956-540X , 1365-246X
    Language: English
    Publisher: Oxford University Press (OUP)
    Publication Date: 2020
    detail.hit.zdb_id: 3042-9
    detail.hit.zdb_id: 2006420-2
    detail.hit.zdb_id: 1002799-3
    SSG: 16,13
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 4
    Online Resource
    Online Resource
    Copernicus GmbH ; 2021
    In:  Safety of Nuclear Waste Disposal Vol. 1 ( 2021-11-10), p. 301-301
    In: Safety of Nuclear Waste Disposal, Copernicus GmbH, Vol. 1 ( 2021-11-10), p. 301-301
    Abstract: Abstract. In the context of selecting and designing a future repository site for nuclear waste, a proper understanding of the host rock's physical behavior is required. One of the fundamental characteristics is the hydraulic diffusivity of the host rock, i.e., the ratio between permeability and storativity. For low-permeability rocks, however, determination of these properties is technically challenging and often time consuming. Among various steady-state and transient methods, the pore pressure oscillation technique has been proven to be an advantageous method for the simultaneous measurement of permeability and storativity for potential host rocks on a laboratory scale. In this contribution, we will introduce the methodological approach and highlight the advantages and disadvantages compared to other methods. Furthermore, we will demonstrate the applicability of this method for clay-rich rocks by presenting our experimental results. Carefully chosen boundary conditions allow us to constrain dependencies of the properties on, e.g., effective stress or bedding orientation with respect to the fluid flow direction. Additionally, this method is practical for measuring the damage-induced changes of permeability and storativity due to differential loading.
    Type of Medium: Online Resource
    ISSN: 2749-4802
    Language: English
    Publisher: Copernicus GmbH
    Publication Date: 2021
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 5
    Online Resource
    Online Resource
    Copernicus GmbH ; 2021
    In:  Safety of Nuclear Waste Disposal Vol. 1 ( 2021-11-10), p. 299-300
    In: Safety of Nuclear Waste Disposal, Copernicus GmbH, Vol. 1 ( 2021-11-10), p. 299-300
    Abstract: Abstract. The testing of low-permeable materials is challenging. Yet, for the disposal of radioactive waste, it is essential, too. This workshop is aimed at gathering ambitious scientists to discuss and to collaborate on their experiences in the laboratory testing of low-permeable materials. The focus here is on the methods: What method is best for what kind of low-permeable host rock (salt/clay) and for what kind of technical barrier material (bentonite/crushed salt)? How can measurement errors be correctly determined? What are the crucial “bottlenecks” in the device setups? How can high porous but low permeable samples best be pre-saturated? How can coupled flow and cumbersome gas traps in the tests be dealt with? What is the best-practice analysis of permeability from pressure decay recordings? Is there a hope of defining a standardized procedure for low-permeability testing? These points will be reflected in the light of radioactive waste disposal and in the need to find a best-practice solution when it comes to eventual evaluation and comparison of potential underground disposal sites.
    Type of Medium: Online Resource
    ISSN: 2749-4802
    Language: English
    Publisher: Copernicus GmbH
    Publication Date: 2021
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 6
    Online Resource
    Online Resource
    Elsevier BV ; 2021
    In:  Engineering Geology Vol. 295 ( 2021-12), p. 106451-
    In: Engineering Geology, Elsevier BV, Vol. 295 ( 2021-12), p. 106451-
    Type of Medium: Online Resource
    ISSN: 0013-7952
    Language: English
    Publisher: Elsevier BV
    Publication Date: 2021
    detail.hit.zdb_id: 1500329-2
    SSG: 19,1
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 7
    Online Resource
    Online Resource
    Copernicus GmbH ; 2022
    In:  Solid Earth Vol. 13, No. 5 ( 2022-05-16), p. 901-915
    In: Solid Earth, Copernicus GmbH, Vol. 13, No. 5 ( 2022-05-16), p. 901-915
    Abstract: Abstract. The way rocks deform under changing stress conditions can be described by different deformation modes, which is fundamental for understanding their rheology. For Opalinus Clay, which is regarded as a potential host rock for nuclear waste, we investigate the failure mode as a function of applied effective stress in laboratory experiments. Therefore, we performed consolidated undrained triaxial tests at different effective consolidation stresses from 2.5 to 16 MPa, in which samples were loaded parallel to bedding, and analysed the deformation structures using ion-beam polishing and electron microscopy. With increasing effective confining stress, the results show a transition from brittle-dominated to more ductile-dominated deformations, localising in distinct shear bands. Both effective stress paths and microstructural analysis indicate a tendency towards less dilation in the shear zones for higher effective stresses. Triaxial test results suggest a non-linear failure envelope. The non-linearity of the failure envelope is associated with decreasing dilation with increasing effective stress accompanied by changes in microstructural deformation processes, which explain the decreasing friction angle. For the first time, we can verify that the observed non-linear failure envelope is due to the gradual transition from brittle- to more ductile-dominated deformation on the microscale controlling the bulk hydro-mechanical behaviour of Opalinus Clay.
    Type of Medium: Online Resource
    ISSN: 1869-9529
    Language: English
    Publisher: Copernicus GmbH
    Publication Date: 2022
    detail.hit.zdb_id: 2545676-3
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
Close ⊗
This website uses cookies and the analysis tool Matomo. More information can be found here...