In:
Powder Diffraction, Cambridge University Press (CUP), Vol. 13, No. 1 ( 1998-03), p. 32-34
Abstract:
Two compounds, [ Co ( NH 3 ) 5 CO 3 ] NO 3 ·1/2 H 2 O (labeled A) and [ Co ( NH 3 ) 4 CO 3 ] NO 3 ·1/2 H 2 O (labeled B), were obtained and characterized by X-ray powder diffraction. The samples were indexed using the programs TREOR90 and DICVOL91 . In a monoclinic setting, the cell parameters are a =7.6661(3) Å, b =9.6212(3) Å, c =7.0725(4) Å, β=106.261(4)°, V =500.78 Å 3 , M 20 =36, F 30 =65 (0.0106, 44) for A and a =10.5623(5) Å, b =22.7304(18) Å, c =7.5174(5) Å, β=91.350(5)°, V =1804.31 Å 3 , M 20 =36, F 30 =82 (0.0071, 52) for B. The space group is probably P 2 1 / m (11) for A and P 2 1 / n (14) for B according to their reflection conditions.
Type of Medium:
Online Resource
ISSN:
0885-7156
,
1945-7413
DOI:
10.1017/S0885715600009726
Language:
English
Publisher:
Cambridge University Press (CUP)
Publication Date:
1998
detail.hit.zdb_id:
2047596-2
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