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  • 1
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2011
    In:  Advanced Materials Research Vol. 194-196 ( 2011-2), p. 1453-1459
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 194-196 ( 2011-2), p. 1453-1459
    Abstract: In order to study the stability of Montmorillonite / Octadecyl trimethyl ammonium complexes in engineering application, the influences of the organic modifier dosage, oscillation intensity, oscillation time, temperature, pH, sodium salt concentration, calcium salt concentration on the stability of Montmorillonite / Octadecyl trimethyl ammonium complexes were systematically investigated. Research results show that the stability of Montmorillonite / Octadecyl trimethyl ammonium complexes slightly reduces with the increases of oscillation intensity, oscillation time and temperature, but the impact isn’t obvious. The more the organic modifier dosage is, the more unstable the Montmorillonite / Octadecyl trimethyl ammonium complexes are. The stability of the Montmorillonite / Octadecyl trimethyl ammonium complexes decreases significantly under the medium conditions of lower or higher pH. The higher the concentration of sodium salts is, the more stable the Montmorillonite / Octadecyl trimethyl ammonium complexes are, but calcium salts are on the contrary.
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2011
    detail.hit.zdb_id: 2265002-7
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  • 2
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2008
    In:  Advanced Materials Research Vol. 58 ( 2008-10), p. 211-224
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 58 ( 2008-10), p. 211-224
    Abstract: Thixotropic gel can be formed in the organic solvents is one of the most important application characteristics of montmorillonite/octadecyl trimethy ammonium chloride complexes. The key factor influencing the formation of gel is the preparation technology, and the posterior disposal process is also an important affecting factor which should be paid more attention to. In the paper, the effects of washing, drying temperature, grind size, activators and the polarity of solvents on the gel viscosity of montmorillonite/octadecyl trimethy ammonium chloride complexes were systematically studied. The research shows that fully washing can elute the octadecyl trimethy ammonium chloride ions or molecula adsorbed on the layer and the edge of montmorillonite crystal, and improve viscosity of gel formed by the complexes. Controlling the drying temperature at the range of 90-100°C and ensuring the complexes with a little interlayer water are favorable for the gel formation of the complexes. When the granularity of the complexes is less than 0.074mm, particles in solvents can fully produce solvation action, solvent swells and strips, and then form the thixotropic organic gel. Using the 95% ethanol as the activator, when its dosage is 5 wt%, its activation effect is better. The stronger the polarity of the dispersing solvent is, the more favorable the formation of the organic gel with higher viscosity is.
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2008
    detail.hit.zdb_id: 2265002-7
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  • 3
    In: Fungal Diversity, Springer Science and Business Media LLC, Vol. 104, No. 1 ( 2020-09), p. 1-266
    Type of Medium: Online Resource
    ISSN: 1560-2745 , 1878-9129
    Language: English
    Publisher: Springer Science and Business Media LLC
    Publication Date: 2020
    detail.hit.zdb_id: 2424484-3
    SSG: 12
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  • 4
    Online Resource
    Online Resource
    Springer Science and Business Media LLC ; 2021
    In:  Acta Pharmacologica Sinica Vol. 42, No. 6 ( 2021-06), p. 909-920
    In: Acta Pharmacologica Sinica, Springer Science and Business Media LLC, Vol. 42, No. 6 ( 2021-06), p. 909-920
    Type of Medium: Online Resource
    ISSN: 1671-4083 , 1745-7254
    Language: English
    Publisher: Springer Science and Business Media LLC
    Publication Date: 2021
    detail.hit.zdb_id: 2088565-9
    SSG: 15,3
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  • 5
    Online Resource
    Online Resource
    Wiley ; 2023
    In:  Rapid Communications in Mass Spectrometry Vol. 37, No. 23 ( 2023-12-15)
    In: Rapid Communications in Mass Spectrometry, Wiley, Vol. 37, No. 23 ( 2023-12-15)
    Abstract: Improving the analytical performance of linear ion traps (LITs) is crucial for the advancement of high‐performance LIT mass spectrometers. In this study, a double resonant excitation method was employed in an asymmetric LIT to achieve high ion unidirectional ejection efficiency and enhanced mass resolution. Methods The asymmetric trapping field was generated by stretching one x electrode with a distance α . The double resonant excitation was achieved by applying an alternating voltage out of phase and a supplementary alternating voltage in phase to the x and y electrode pairs of the LIT, respectively. Numerical simulations of ion trajectories were performed to validate the effectiveness of this method. Results The mass resolution of the asymmetric LIT with double resonant excitation could be improved to ~3800, which was over two times compared to that with only dipolar resonant excitation, while both reached ~90% in ion unidirectional ejection efficiency. Conclusions By employing the double resonant excitation method, the mass resolution could be improved significantly in the asymmetric LIT, while maintaining a considerably high ion unidirectional ejection efficiency. This method might provide a general solution for enhancing ion detection efficiency and mass resolution of LIT mass spectrometers.
    Type of Medium: Online Resource
    ISSN: 0951-4198 , 1097-0231
    URL: Issue
    Language: English
    Publisher: Wiley
    Publication Date: 2023
    detail.hit.zdb_id: 2002158-6
    detail.hit.zdb_id: 58731-X
    SSG: 11
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  • 6
    In: Frontiers in Psychology, Frontiers Media SA, Vol. 14 ( 2023-9-15)
    Abstract: This study aimed to revise and examine the reliability and validity of the Chinese version of the Athens Insomnia Scale for Non-clinical Application (AIS-NCA) among Chinese athletes. Additionally, the study tested the scale in non-athlete individuals with similar sleep management practices to further analyze its cultural specificity among Chinese athletes and make preliminary inferences about its applicability in other Chinese populations. Methods Four hundred twenty-six Chinese professional athletes and 779 high school students participated in this research. Both athletes and students were divided into two parallel groups for exploratory and confirmatory factor analyses. Additionally, three athlete samples and one student sample were established for reliability and validity assessments. Among athletes, the Pittsburgh Sleep Quality Index, the Epworth Sleepiness Scale, the Athlete Sleep Screening Questionnaire, and the Warwick-Edinburgh Mental Well-Being Scale were employed to evaluate convergent and discriminant validity. Re-test reliability was evaluated at intervals of 1 and 2 weeks. In the case of students, convergent and discriminant validity were tested using the Pittsburgh Sleep Quality Index and the General Self-Efficacy Scale, with re-test reliability assessed at two-week intervals. Results The Chinese version of the AIS-NCA consists of six items, categorized into two dimensions: sleep problems and daytime functioning. This structure explained 65.08% (athletes) and 66.22% (students) of the variance. Confirmatory factor analysis revealed good model fit, with values of χ 2 / df  = 2.217, CFI = 0.975, AGFI = 0.929, TLI = 0.953, and RMSEA = 0.076 among athletes, and χ 2 / df  = 3.037, CFI = 0.979, AGFI = 0.947, TLI = 0.961, and RMSEA = 0.072 among students. The scale demonstrated a reasonable degree of measurement invariance. The overall scale and two subscales exhibited strong reliability and validity among athletes. Similar results in terms of reliability and validity were also observed within the student sample. Conclusion The Chinese version of the AIS-NCA shows promise as an assessment tool for evaluating the sleep quality of Chinese athletes. It effectively captures both sleep-related concerns and daytime functionality within the athlete population. The scale demonstrates solid reliability and validity in professional athletes and holds potential for application across various other demographic groups in China.
    Type of Medium: Online Resource
    ISSN: 1664-1078
    Language: Unknown
    Publisher: Frontiers Media SA
    Publication Date: 2023
    detail.hit.zdb_id: 2563826-9
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  • 7
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2010
    In:  Advanced Materials Research Vol. 158 ( 2010-11), p. 25-34
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 158 ( 2010-11), p. 25-34
    Abstract: The structure and thermal property of organomontmorillonite (OM) were studied by X-ray diffraction (XRD), differential thermal analysis (DTA), and thermalgravimetric analysis (TGA).Based on the thermal property of OM, a new method for quantitative characterization of the alkyl-ammonium adsorbed in the layers was established, and the influence of adsorption amount on the viscosity of OM gel was examined. Changes in the basal spacing of OMs and Na-montmorillonite (Na-mont) indicated that alky-ammonium ions intercalated into the montmorillonite layers. TGA results showed that OM and Na-mont had different thermal property, Na-mont held more free water in the layers. The intercalated alkyl-ammonium in OMs decomposed at the temperature of 230~480°C. Effective dosage (DOSeffective) has significant influence on the viscosity of OM gel. Under the optimal DOSeffective(1.1~1.3CEC), the alkyl-ammonium cations can fully cover the exchangeable site in the layers, then the “card-house” structure formed. Structure of the alkyl-ammonium cations determines the intercalation efficiency, the longer the carbon chain, the higher the intercalation efficiency. The intercalation efficiency has no evident correlativity with the viscosity; however, structure of the alkyl-ammonium cations determines their arrangement in the layers.
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2010
    detail.hit.zdb_id: 2265002-7
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  • 8
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2010
    In:  Advanced Materials Research Vol. 158 ( 2010-11), p. 248-255
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 158 ( 2010-11), p. 248-255
    Abstract: Al3+/clay ratio is one of the important factors influencing microstructure of Al-pillared montmorillonite. Microstructure variation laws of Al-pillared montmorillonite prepared under the condition of different Al3+/clay ratio are systematically studied by XRD, FTIR, specific surface area and pore size analysis. The results show that the interlayer spacing and BET specific surface area of Al-pillared montmorillonite are remarkably affected by the Al3+/clay ratio. The interlayer spacing d(001) value and BET specific surface area of Al-pillared montmorillonite increase firstly and then decrease with the increases of the Al3+/clay ratio, and they reach to maximum when the Al3+/clay ratio is 10mmol/g. Besides, the BJH porous volume distribution of Al-pillared montmorillonite is the most probable distribution, and the most probable pore size is about 2 nm, which is attributed to mesopore. The porous structure of hydroxy-Al pillared montmorillonite is characterized as parallel plate slit or “house-of-cards” wedge-shaped pore which is formed by novel meso-microporous delaminated structure and fragments. With the increase of the Al3+/clay ratio, BJH total porous volume and mesoporous volume of hydroxy-Al pillared montmorillonite decreases, while the proportion of microporous volume in the total porous volume increases. The proportion of microporous specific surface area of all the hydroxy-Al pillared montmorillonite samples is about 62% and is much larger than that of Na-M and those of mesopore and macropore, indicating the main action of intercalation of hydroxy-Al pillaring solution into montmorillonite interlayer is to increase the micropore amount.
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2010
    detail.hit.zdb_id: 2265002-7
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  • 9
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2010
    In:  Advanced Materials Research Vol. 158 ( 2010-11), p. 273-280
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 158 ( 2010-11), p. 273-280
    Abstract: In order to study the phase of Fe and Ti in a beach placer , different methods such as the X-ray diffraction analysis, chemical analysis, scanning electron microscopic , electron probe microanalysis are used to study the characteristics of the beach placer . The research results show the major metallic mineral in the beach placer is titanic magnetite, EDS and energy spectrum map features of which indicate that the vast majority of titanic magnetite contain a certain amount of Ti , the two elements of Fe and Ti take on closely symbiosis and distribute more evenly in titanic magnetite. The Ti exists in the Magnetite lattice in form of isomorphism. The theoretical highest grade of Fe and Ti in the separated Magnetic concentrate are 66.02per cent and 4.86 per cent respectively. In addition, the beach placer contains a small quantity of Ilmenite which is hysterogenic and exists in the form of fine solid solution separation structure in the titanic magnetite
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2010
    detail.hit.zdb_id: 2265002-7
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  • 10
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2012
    In:  Advanced Materials Research Vol. 454 ( 2012-1), p. 305-309
    In: Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 454 ( 2012-1), p. 305-309
    Abstract: Using Octadecyltrimethylammonium cations with long carbon chain to modify calcium montmorillonite samples, the adsorption properties of different dyes on montmorillonite before and after modification were investigated. Results showed that the basic dye of methylene blue was easily adsorbed by natual calcium montmorillonite, while the adsorption ability for acid blue and neutral blue was greatly improved when it was organically modified, and the adsorption amount increased with the increasing of modifier dosage. The adsorption ratio was influnced by reaction time, the temperature and the solution’s pH value. It suggested that the adsorption balance time was about 60min; higher temperature was good for acid blue adsorbed on organic montmorillonite, but neutral blue’s adsorption amount was greater at the room temperature; the optimum pH was 9 for methylene blue adsorption, while low pH was better for acid blue and neutral blue adsorption.
    Type of Medium: Online Resource
    ISSN: 1662-8985
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2012
    detail.hit.zdb_id: 2265002-7
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