In:
Acta Crystallographica Section E Crystallographic Communications, International Union of Crystallography (IUCr), Vol. 71, No. 7 ( 2015-07-01), p. o525-o526
Abstract:
The title molecular salt, C 15 H 22 N + ·Cl − , arose as an unexpected product of the reaction between aniline and melanol in the presence of HCl. The central heterocyclic ring has a half-chair conformation and the five-membered ring has an envelope conformation, with the C atom linked to the N atom as the flap. In the crystal, the ions are linked by N—H...Cl hydrogen bonds, generating chains propagating in the [100] direction. The crystal studied was a merohedral twin with a 0.64 (3):0.36 (3) domain ratio.
Type of Medium:
Online Resource
ISSN:
2056-9890
DOI:
10.1107/S2056989015011858
DOI:
10.1107/S2056989015011858/hb7450sup1.cif
DOI:
10.1107/S2056989015011858/hb7450Isup2.hkl
DOI:
10.1107/S2056989015011858/hb7450Isup3.cml
Language:
Unknown
Publisher:
International Union of Crystallography (IUCr)
Publication Date:
2015
detail.hit.zdb_id:
2843762-7
detail.hit.zdb_id:
2041947-8
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