GLORIA

GEOMAR Library Ocean Research Information Access

Your email was sent successfully. Check your inbox.

An error occurred while sending the email. Please try again.

Proceed reservation?

Export
Filter
Material
Language
  • 1
    In: Journal of Applied Physics, AIP Publishing, Vol. 117, No. 16 ( 2015-04-28)
    Abstract: In the recently developed technique of X-ray Birefringence Imaging, molecular orientational order in anisotropic materials is studied by exploiting the birefringence of linearly polarized X-rays with energy close to an absorption edge of an element in the material. In the experimental setup, a vertically deflecting high-resolution double-crystal monochromator is used upstream from the sample to select the appropriate photon energy, and a horizontally deflecting X-ray polarization analyzer, consisting of a perfect single crystal with a Bragg reflection at Bragg angle of approximately 45°, is placed downstream from the sample to measure the resulting rotation of the X-ray polarization. However, if the experiment is performed on a synchrotron bending-magnet beamline, then the elliptical polarization of the X-rays out of the electron orbit plane affects the shape of the output beam. Also, because the monochromator introduces a correlation between vertical position and photon energy to the X-ray beam, the polarization analyzer does not select the entire beam, but instead selects a diagonal stripe, the slope of which depends on the Bragg angles of the monochromator and the polarization analyzer. In the present work, the final background intensity distribution is calculated analytically because the phase space sampling methods normally used in ray traces are too inefficient for this setup. X-ray Birefringence Imaging data measured at the Diamond Light Source beamline B16 agree well with the theory developed here.
    Type of Medium: Online Resource
    ISSN: 0021-8979 , 1089-7550
    Language: English
    Publisher: AIP Publishing
    Publication Date: 2015
    detail.hit.zdb_id: 220641-9
    detail.hit.zdb_id: 3112-4
    detail.hit.zdb_id: 1476463-5
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 2
    Online Resource
    Online Resource
    American Chemical Society (ACS) ; 2015
    In:  The Journal of Physical Chemistry Letters Vol. 6, No. 3 ( 2015-02-05), p. 561-567
    In: The Journal of Physical Chemistry Letters, American Chemical Society (ACS), Vol. 6, No. 3 ( 2015-02-05), p. 561-567
    Type of Medium: Online Resource
    ISSN: 1948-7185 , 1948-7185
    Language: English
    Publisher: American Chemical Society (ACS)
    Publication Date: 2015
    detail.hit.zdb_id: 2522838-9
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 3
    In: Journal of Synchrotron Radiation, International Union of Crystallography (IUCr), Vol. 27, No. 5 ( 2020-09-01), p. 1438-1446
    Abstract: B21 is a small-angle X-ray scattering (SAXS) beamline with a bending magnet source in the 3 GeV storage ring at the Diamond Light Source Ltd synchrotron in the UK. The beamline utilizes a double multi-layer monochromator and a toroidal focusing optic to deliver 2 × 10 12 photons per second to a 34 × 40 µm (FWHM) focal spot at the in-vacuum Eiger 4M (Dectris) detector. A high-performance liquid chromatography system and a liquid-handling robot make it possible to load solution samples into a temperature-controlled in-vacuum sample cell with a high level of automation. Alternatively, a range of viscous or solid materials may be loaded manually using a range of custom sample cells. A default scattering vector range from 0.0026 to 0.34 Å −1 and low instrument background make B21 convenient for measuring a wide range of biological macromolecules. The beamline has run a full user programme since 2013.
    Type of Medium: Online Resource
    ISSN: 1600-5775
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2020
    detail.hit.zdb_id: 2021413-3
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 4
    Online Resource
    Online Resource
    American Chemical Society (ACS) ; 1960
    In:  Journal of the American Chemical Society Vol. 82, No. 24 ( 1960-12), p. 6420-6420
    In: Journal of the American Chemical Society, American Chemical Society (ACS), Vol. 82, No. 24 ( 1960-12), p. 6420-6420
    Type of Medium: Online Resource
    ISSN: 0002-7863 , 1520-5126
    RVK:
    Language: English
    Publisher: American Chemical Society (ACS)
    Publication Date: 1960
    detail.hit.zdb_id: 1472210-0
    detail.hit.zdb_id: 3155-0
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 5
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2008
    In:  Journal of Synchrotron Radiation Vol. 15, No. 6 ( 2008-11-01), p. 584-592
    In: Journal of Synchrotron Radiation, International Union of Crystallography (IUCr), Vol. 15, No. 6 ( 2008-11-01), p. 584-592
    Type of Medium: Online Resource
    ISSN: 0909-0495
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2008
    detail.hit.zdb_id: 2021413-3
    SSG: 13
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 6
    Online Resource
    Online Resource
    Springer Science and Business Media LLC ; 2017
    In:  MRS Bulletin Vol. 42, No. 06 ( 2017-06), p. 424-429
    In: MRS Bulletin, Springer Science and Business Media LLC, Vol. 42, No. 06 ( 2017-06), p. 424-429
    Abstract: The use of crystals other than silicon for x-ray optics is becoming more common for many challenging experiments such as resonant inelastic x-ray scattering and nuclear resonant scattering. As more—and more specialized—spectrometers become available at many synchrotron radiation facilities, interest in pushing the limits of experimental energy resolution has increased. The potentially large improvements in resolution and efficiency that nonsilicon optics offer are beginning to be realized. This article covers the background and state of the art for nonsilicon crystal optics with a focus on a resolution of 10 meV or better, concentrating on compounds that form trigonal crystals, including sapphire, quartz, and lithium niobate, rather than the more conventional cubic materials, including silicon, diamond, and germanium.
    Type of Medium: Online Resource
    ISSN: 0883-7694 , 1938-1425
    Language: English
    Publisher: Springer Science and Business Media LLC
    Publication Date: 2017
    detail.hit.zdb_id: 2749565-6
    detail.hit.zdb_id: 2136359-6
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 7
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2003
    In:  Journal of Applied Crystallography Vol. 36, No. 6 ( 2003-12-01), p. 1432-1439
    In: Journal of Applied Crystallography, International Union of Crystallography (IUCr), Vol. 36, No. 6 ( 2003-12-01), p. 1432-1439
    Abstract: A Michelson interferometer for X-rays of wavelength ∼1 Å has been proposed to test the temporal coherence of FEL radiation. Such a device has been made at HASYLAB from a silicon single crystal. It is based on the BBB interferometer of Bonse and Hart. One of its mirrors can be pushed by a piezo to introduce the desired beam path difference. For the preliminary tests described in this paper, the crystal was also equipped with an LLL interferometer to check the quality of the crystal and of its preparation. The rotation of a phase-shifting object (a Plexiglas plate) in one of the LLL's beam paths has been found to produce a fringe pattern which can be shown to yield the phase-shifting material's index of refraction. The interferometer crystal's front section was held fixed with a compression spring. At the same time, the interferometer was bathed in viscous silicone oil to reduce vibrations.
    Type of Medium: Online Resource
    ISSN: 0021-8898
    RVK:
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2003
    detail.hit.zdb_id: 2020879-0
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 8
    In: Journal of Synchrotron Radiation, International Union of Crystallography (IUCr), Vol. 26, No. 1 ( 2019-01-01), p. 45-51
    Abstract: The tangential curvature of actively bent X-ray mirrors at synchrotron radiation and X-ray free-electron laser (XFEL) facilities is typically only changed every few hours or even days. This operation can take tens of minutes for active optics with multiple bending actuators and often requires expert guidance using in situ monitoring devices. Hence, the dynamic performance of active X-ray optics for synchrotron beamlines has historically not been exploited. This is in stark contrast to many other scientific fields. However, many areas of synchrotron radiation and XFEL science, including macromolecular crystallography, could greatly benefit from the ability to change the size and shape of the X-ray beam rapidly and continuously. The advantages of this innovative approach are twofold: a large reduction in the dead time required to change the size of the X-ray beam for different-sized samples and the possibility of making multiple changes to the beam during the measurement of a single sample. In the preceding paper [Part I; Alcock, Nistea, Signorato & Sawhney (2019), J. Synchrotron Rad. 26 , 36–44], which accompanies this article, high-speed visible-light Fizeau interferometry was used to identify the factors which influence the dynamic bending behaviour of piezoelectric bimorph deformable X-ray mirrors. Building upon this ex situ metrology study, provided here is the first synchrotron radiation beamline implementation of high-speed adaptive X-ray optics using two bimorphs operating as a Kirkpatrick–Baez pair. With optimized substrates, novel opto-mechanical holders and a next-generation high-voltage power supply, the size of an X-ray beam was rapidly and repeatedly switched in 〈 10 s. Of equal importance, it is also shown that compensation of piezoelectric creep ensures that the X-ray beam size remains stable for more than 1 h after making a major change. The era of high-speed adaptive X-ray optics for synchrotron radiation and XFEL beamlines has begun.
    Type of Medium: Online Resource
    ISSN: 1600-5775
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2019
    detail.hit.zdb_id: 2021413-3
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 9
    In: Journal of Synchrotron Radiation, International Union of Crystallography (IUCr), Vol. 25, No. 5 ( 2018-09-01), p. 1556-1564
    Abstract: A description of the technical and design details of a scanning four-bounce crystal monochromator that has recently been commissioned for the Versatile X-ray Absorption Spectroscopy (XAS) beamline at Diamond Light Source is presented. This device consists of two independent rotary axes of unique design which are synchronized using a multiple read-head encoder system. This monochromator is shown to be capable of maintaining the flux throughput of the Bragg axes without the need of any external feedback mechanism from 4 to 20 keV. The monochromator is currently equipped with cryogenically cooled crystals with the upstream axis consisting of two independent Si(111) crystals and a pair of channel-cut crystals in the downstream axis. The possibility of installing an additional Si(311) crystal-set to extend the energy range to 34 keV is incorporated into the preliminary design of the device. Experimental data are presented showing the exceptional mechanical stability and repeatability of the monochromator axes.
    Type of Medium: Online Resource
    ISSN: 1600-5775
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2018
    detail.hit.zdb_id: 2021413-3
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 10
    Online Resource
    Online Resource
    IOP Publishing ; 2022
    In:  Journal of Physics: Conference Series Vol. 2380, No. 1 ( 2022-12-01), p. 012055-
    In: Journal of Physics: Conference Series, IOP Publishing, Vol. 2380, No. 1 ( 2022-12-01), p. 012055-
    Abstract: With brighter synchrotron sources, automated sample changers, and faster detectors, there is a strong scientific need for rapid and precise variation of the X-ray beam profile, rather than the “set and forget” operation of years past. Piezoelectric bimorph deformable mirrors already allow quick beam profile changes without the heat generation and wear of mechanical devices. Now, their early technological limitations – excessively constraining holders, progressive “junction effect” distortion, and communication bottlenecks with power supplies – are being overcome by a collaboration of scientists and engineers both in industry and at Diamond Light Source. A new generation of bimorph mirrors maintains a stable figure over extended periods of operation. Improved holders and flexible electrical connectors are greatly reducing the mechanical strain imparted to bimorphs, thereby improving their speed, accuracy, and stability. A more sophisticated high voltage power supply has on-board signal processing capacity, allowing large focusing changes within seconds and providing programmable time-varying voltage profiles to counteract piezoelectric creep. The communication between beamline systems and power supplies is being freed of bottlenecks and now runs stably up to 1 Hz. Early tests have already shown that bimorph mirrors can repeatedly switch the size of an X-ray beam in well under 10 seconds. Bimorph mirrors at synchrotron beamlines are now growing beyond the largely static operation of the past and gaining a new dynamism through development projects that are now well advanced. We report on how these endeavours will make it easier for beamlines to utilise the full potential of bimorph mirrors.
    Type of Medium: Online Resource
    ISSN: 1742-6588 , 1742-6596
    Language: Unknown
    Publisher: IOP Publishing
    Publication Date: 2022
    detail.hit.zdb_id: 2166409-2
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
Close ⊗
This website uses cookies and the analysis tool Matomo. More information can be found here...