In:
Advances in X-ray Analysis, Cambridge University Press (CUP), Vol. 15 ( 1971), p. 102-113
Abstract:
The instrumentation and software for performing X-ray intensity measurements with a paper tape controlled diffractometer are described. The hardware includes two addressable axis positioners which control Slo-Syn stepping motors on the 2θ and ω) axes of the diffractometer, an addressable scaler-timer, a multiaxis programmer and a Teletype, in addition to the normal counting electronics. This system may be manually controlled with front panel switches or with instructions entered on the Teletype. In the automatic off-line mode instructions for motor speed, motor direction, starting angle, final angle, angular increment and scaler preset (time or counts) punched on paper tape are read and executed in sequence. A Teletype output of 2θ and ω angles, time and counts is obtained at each step. This off-line system was used for the measurement of austenite in H12 hot work die steel austenitized at various conditions and which contained a maximum of 13% austenite. A helium chamber was used to extend the limit of detection to 0.4% austenite. The X-ray analysis involved measuring the areas of the (200) austenite diffraction line and the (200) martensite line. For each of these lines, the system was programmed to integrate the counts over angular intervals corresponding to a low-angle background, the peak and a high-angle background using the ability of the axis positioner to stop the scaler-timer at the end of each angular interval. The additional capability of slewing rapidly between the various diffraction lines reduced the time required for automatic data collection. The present off-line system can be used to simplify other types of X-ray diffraction analysis such as residual stress and microstrain/particle size determinations, since the manual data handling can be eliminated with the computer compatible punched paper tape output. Future development of this instrumentation includes direct computer control of the diffractometer and computerized data reduction, with the advantage of a paper tape back-up system.
Type of Medium:
Online Resource
ISSN:
0376-0308
,
2631-3626
DOI:
10.1154/S0376030800010831
Language:
English
Publisher:
Cambridge University Press (CUP)
Publication Date:
1971
detail.hit.zdb_id:
2498440-1
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