In:
European Journal of Organic Chemistry, Wiley, Vol. 2017, No. 44 ( 2017-12), p. 6483-6485
Abstract:
An efficient flow system was constructed for the synthesis of [6,6]‐phenyl‐C 61 ‐butyric acid methyl ester (PCBM); the process involved flow [2+1] addition of C 60 and subsequent flow photoisomerization of the resulting fulleroid to PCBM by using a flow photoreactor in combination with an Na lamp. With the present flow system, a scalable synthesis of PCBM (0.79 g/3.3 h) was achieved by continuous operation for 3.3 h.
Type of Medium:
Online Resource
ISSN:
1434-193X
,
1099-0690
DOI:
10.1002/ejoc.v2017.44
DOI:
10.1002/ejoc.201700745
Language:
English
Publisher:
Wiley
Publication Date:
2017
detail.hit.zdb_id:
1475010-7
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