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  • Phthalocyaninato complexes  (3)
  • Industrial Chemistry and Chemical Engineering  (2)
  • 1
    Electronic Resource
    Electronic Resource
    Soluble (Phthalocyaninato)ruthenium(II) Phosphane Complexes (1993)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 126 (1993), S. 2565-2566 
    Details
    ISSN: 0009-2940
    Keywords: Phthalocyaninato complexes ; Ruthenium complexes ; Phosphanes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Hitherto unknown ruthenium phthalocyanine complexes with phosphane ligands - PcRu(PEt2Ph)2 (1) and PcRu(PPh3)2 (2) - soluble in common organic solvents were prepared. Two methods were used for their synthesis: 1) Reaction of phthalonitrile with [Ru2Cl3(PEt2Ph)6]Cl in n-pentanol in the presence of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) and 2) reaction of PcRu with the corresponding phosphanes. The products 1 and 2 were characterized by their IR, UV/Vis, FD-MS, and 1H-NMR data.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19931261136
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  • 2
    Electronic Resource
    Electronic Resource
    Synthesis and Characterization of Nitrido(tetra-tert-butylphthalocyaninato)- rhenium(V) and Nitrido(phthalocyaninato)rhenium(V) (1994)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 127 (1994), S. 1681-1685 
    Details
    ISSN: 0009-2940
    Keywords: Rhenium(V), nitrido(tetra-tert-butylphthalocyaninato)- ; Rhenium(V), nitrido(phthalocyaninato)- ; Phthalocyaninato complexes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: 4-tert-Butylphthalodinitrile (1) reacts with ammonium perrhenate, NH4ReO4, to yield nitrido(tetra-tert-butylphthalocyaninato)rhenium(V), (tBu)4PcReN (2), which is characterized by IR, UV/Vis, CV, MS, 1H and 13C NMR, and elemental analysis. It shows good solubility in common organic solvents. In solution 2 is assumed to be monomeric whereas in the solid state also dimers or higher aggregates are present. From the NMR spectra it is concluded that different constitutional isomers of 2 are formed but not in the expected ratio of a statistical distribution. By analogy with 2, the already known nitrido(phthalocyaninato)rhenium(V), PcReN (3), is prepared for comparison.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19941270919
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  • 3
    Electronic Resource
    Electronic Resource
    Synthesis and Properties of (Tetra-tert-butylphthalocyaninato)ruthenium(II) and (Tetra-tert-butyl-2,3-naphthalocyaninato)ruthenium(II) (1995)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 128 (1995), S. 929-933 
    Details
    ISSN: 0009-2940
    Keywords: (Phthalocyaninato)ruthenium, soluble tert-butyl-substituted ; (2,3-Naphthalocyaninato)ruthenium, tert-butyl-substituted ; Ruthenium complexes ; Phthalocyaninato complexes ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The first synthesis of pure tert-butyl-substituted (phthalocyaninato)- and (2,3-naphthalocyaninato)ruthenium [(tBu)4-MacRu] by thermal decomposition of (tBu)4MacRu(L)2 (L = 3-chloropyridine, ammonia) is described. The compounds were characterized by UV/Vis, IR, and NMR measurements.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19951280913
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  • 4
    Electronic Resource
    Electronic Resource
    Synthesis of Oligomeric Axially Bridged Ruthenium Phthalocyanines and 2,3-Naphthalocyanines (1996)
    New York, NY [u.a.] : Wiley-Blackwell
    Applied Organometallic Chemistry 10 (1996), S. 649-660 
    Details
    ISSN: 0268-2605
    Keywords: naphthalocyanine ; ruthenium ; bridged ; oligomers ; solid state ; NMR ; conductivity ; Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Bridged 2,3-naphthalocyaninatoruthenium oligomers {[MacRu(L)]n} were synthesized and characterized using solid-state methods. For comparison, soluble t-butyl substituted phthalocyaninatoruthenium oligomers were prepared and their chain length examined by 1H NMR spectroscopy. The powder conductivities of all bridged compounds ([MacRu(L)]n) were measured and the dependence of the conductivities on the bridging ligands is discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Third-order Nonlinear Optical Properties of Octa-substituted Metal-free Phthalocyanine Thin Films (1996)
    New York, NY [u.a.] : Wiley-Blackwell
    Applied Organometallic Chemistry 10 (1996), S. 661-664 
    Details
    ISSN: 0268-2605
    Keywords: third-order optical nonlinear properties ; optical susceptibility; phthalocyanine ; third-harmonic generation ; Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Third-order nonlinear optical susceptibility, χ(3) of symmetrically octa-substituted metal-free phthalocyanine thin films measured by the third-harmonic generation technique are reported. The metal-free phthalocyanine has been found to show a χ(3) (-3ω; ω,ω, ω) value as large as 7.73×10-12 esu at 1.80 μm. The figure of merit, χ(3)/α, was estimated to be 4.17×1017 esu cm at 1.05 μm and 6.97×1016 esu cm at 1.65 μm. Both linear and third-order optical properties of liquid-crystalline metal-free phthalocyanines are discussed
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
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