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  • 1-Nitroso-3-nitro-1,3-diazacycloalkanes  (1)
  • 19F NMR  (1)
  • 1
    Electronic Resource
    Electronic Resource
    NMR coupling of 13C and 19F with 14N in nitro compounds (1990)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 28 (1990), S. 16-20 
    Details
    ISSN: 0749-1581
    Keywords: Nitro compounds ; 13C NMR ; 14N NMR ; 19F NMR ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The 13C and 14N NMR spectra of a variety of highly nitrated aliphatic, aromatic and heterocyclic compounds were obtained. The proton decoupled 13C peaks of the nitro-substituted carbons in most of these compounds were split into the multiplets expected for coupling with spin 1 nuclei with negligible quadrupolar broadening. In addition, the 19F spectra of some fluoronitroaliphatic compounds showed that the 19F signals were also split into the expected multiplets from coupling with the 14N of the nitro groups.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260280105
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    1,3-dinitroso-, 1-nitroso-3-nitro-, and 1,3-dinitro-1,3-diazacycloalkanes. A multinuclear NMR studySee Ref. 1. (1988)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 26 (1988), S. 95-103 
    Details
    ISSN: 0749-1581
    Keywords: 1,3-Dinitroso-1,3-diazacycloalkanes ; 1-Nitroso-3-nitro-1,3-diazacycloalkanes ; 1,3-Dinitro-1,3-diazacycloalkanes ; Multinuclea gHNMR ; Rotamer populations ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A series of five-, six-, and seven-membered 1,3-dinitroso-, 1-nitroso-3-nitro-, and 1,3-dinitro-1,3-diazacycloalkanes were investigated by 1H, 13C, and 15N NMR spectroscopy. Hindered rotation of the nitrosamine group leads to the existence of rotational isomers. The relative populations of rotamer forms are determined by steric and electrostatic interactions between nitroso groups and the remainder of the molecule, and by the size of the ring.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260260202
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    Paper (German National Licenses)
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