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  • International Union of Crystallography (IUCr)  (9)
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  • International Union of Crystallography (IUCr)  (9)
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  • 1
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2018
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 74, No. 5 ( 2018-09-01), p. 586-594
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 74, No. 5 ( 2018-09-01), p. 586-594
    Abstract: The real part of the dispersion surface in X-ray dynamical diffraction in the Laue case for perfect crystals is analysed using a Riemann surface. In the conventional two-beam approximation, each branch or wing of the dispersion surface is specified by one sheet of the Riemann surface. The characteristic features of the dispersion surface are analytically revealed using four parameters, which are the real and imaginary parts of two quantities that specify the degree of departure from the exact Bragg condition and the reflection strength. The present analytical method is generally applicable, irrespective of the magnitudes of the parameters with no approximation. Characteristic features of the dispersion surface are also revealed by geometrical considerations with respect to the Riemann surface.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2018
    detail.hit.zdb_id: 2020844-3
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  • 2
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2016
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 72, No. 4 ( 2016-07-01), p. 472-479
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 72, No. 4 ( 2016-07-01), p. 472-479
    Abstract: Continuing the work described in the previous paper [Saka (2016). Acta Cryst. A 72 , 338–348], the dynamical theory for perfect crystals in the Bragg case is reformulated using the Riemann surface. In particular, diffraction under resonant scattering conditions is investigated. The characteristic features of the dispersion surface and the rocking curve are analytically revealed using four parameters, which are the real and imaginary parts of two quantities specifying the degree of departure from the exact Bragg conditions and the reflection strength. Characteristic properties that have been deduced through numerical analysis are derived analytically using these four parameters. Visualization of the geometric relationships between the four parameters on the Riemann surface is useful for understanding many properties such as symmetry and sharpness of the rocking curve under special conditions. Therefore, employing the Riemann surface is instructive for numerical analysis and useful for understanding dynamical diffraction in the Bragg case.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2016
    detail.hit.zdb_id: 2020844-3
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  • 3
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2018
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 74, No. 5 ( 2018-09-01), p. 578-585
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 74, No. 5 ( 2018-09-01), p. 578-585
    Abstract: The direction of energy flow for Bloch waves during X-ray dynamical diffraction in perfect crystals is investigated. The energy flow is spread uniformly within the Borrmann fan in the conventional Laue case where the imaginary part of the crystal structure factor is much smaller than the real part. However, when the imaginary part is large, as in the case of X-rays with energies close to the absorption edge for single atoms in crystals, the energy flow direction is found to be restricted, and the results are discussed in relation to the Bragg case.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2018
    detail.hit.zdb_id: 2020844-3
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  • 4
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2003
    In:  Journal of Applied Crystallography Vol. 36, No. 2 ( 2003-04-01), p. 249-254
    In: Journal of Applied Crystallography, International Union of Crystallography (IUCr), Vol. 36, No. 2 ( 2003-04-01), p. 249-254
    Abstract: A very sensitive method to detect long-range strain in otherwise perfect crystalline materials is presented. In this method, a specimen is set vertically in a diffraction apparatus under the symmetrical Laue condition, in which the scattering vector is horizontal. The specimen is then rotated along the scattering vector, with the Bragg condition being kept satisfied. Experiments were carried out using Si crystals of 714 µm thickness with X-rays of 0.4 Å wavelength. The Si crystals were strained by scratching the surface with a glass-cutter. A characteristic behaviour of the integrated intensities was observed. When the specimens were rotated in the opposite direction, the integrated intensities were different and sharply enhanced integrated intensities of the higher order reflections were observed when the specimens were rotated from their initial vertical positions. The observed results can be explained using the dynamical theory of X-ray diffraction for distorted crystals, with the assumption that the specimens were bent along an axis lying on the specimen surface. This method of rotating the crystal along the scattering vector is a very sensitive method to detect minute strains induced by device fabrication processes. The detection limit for the presented specimen is estimated to be equivalent to a uniform bending with a radius of curvature of 7000 m.
    Type of Medium: Online Resource
    ISSN: 0021-8898
    RVK:
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2003
    detail.hit.zdb_id: 2020879-0
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  • 5
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2016
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 72, No. 3 ( 2016-05-01), p. 338-348
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 72, No. 3 ( 2016-05-01), p. 338-348
    Abstract: The dynamical theory for perfect crystals in the Laue case was reformulated using the Riemann surface, as used in complex analysis. In the two-beam approximation, each branch of the dispersion surface is specified by one sheet of the Riemann surface. The characteristic features of the dispersion surface are analytically revealed using four parameters, which are the real and imaginary parts of two quantities specifying the degree of departure from the exact Bragg condition and the reflection strength. By representing these parameters on complex planes, these characteristics can be graphically depicted on the Riemann surface. In the conventional case, the absorption is small and the real part of the reflection strength is large, so the formulation is the same as the traditional analysis. However, when the real part of the reflection strength is small or zero, the two branches of the dispersion surface cross, and the dispersion relationship becomes similar to that of the Bragg case. This is because the geometrical relationships among the parameters are similar in both cases. The present analytical method is generally applicable, irrespective of the magnitudes of the parameters. Furthermore, the present method analytically revealed many characteristic features of the dispersion surface and will be quite instructive for further numerical calculations of rocking curves.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2016
    detail.hit.zdb_id: 2020844-3
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  • 6
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2020
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 76, No. 2 ( 2020-03-01), p. 132-136
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 76, No. 2 ( 2020-03-01), p. 132-136
    Abstract: Formulations are given for the intensities of transmitted and diffracted waves in the Laue case of a perfect crystal. This is applicable irrespective of the magnitudes of both the real and imaginary parts of the Fourier components of the crystal polarizability. The phase shift of the Pendellösung oscillations of the transmitted and diffracted waves is analyzed in detail for a symmetrical Laue case. The phase is determined to shift continuously from out of phase to in phase for absorbing crystals.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2020
    detail.hit.zdb_id: 2020844-3
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  • 7
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2012
    In:  Journal of Applied Crystallography Vol. 45, No. 3 ( 2012-06-01), p. 496-502
    In: Journal of Applied Crystallography, International Union of Crystallography (IUCr), Vol. 45, No. 3 ( 2012-06-01), p. 496-502
    Abstract: Long-range strain in nearly perfect crystalline materials can be detected by dynamical X-ray diffraction. Long-range strain due to uniform bending or torsion is undetectable by conventional methods when the specimen is vertical in a symmetrical Laue setting, but it can be detected by rotating the specimen along the scattering vector. This method is applied to Si devices for a resonating torsion mirror in a micro-electromechanical system. X-ray transmission topography clearly reveals local strain concentrations as enhancements or reductions in the diffraction intensity where non-uniform strain exists. In conjunction with reflection plane-wave topography, a model of local strain is proposed and the strain qualitatively analysed.
    Type of Medium: Online Resource
    ISSN: 0021-8898
    RVK:
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2012
    detail.hit.zdb_id: 2020879-0
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  • 8
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2005
    In:  Journal of Applied Crystallography Vol. 38, No. 6 ( 2005-12-01), p. 958-963
    In: Journal of Applied Crystallography, International Union of Crystallography (IUCr), Vol. 38, No. 6 ( 2005-12-01), p. 958-963
    Abstract: A very sensitive method to detect long-range strain in otherwise perfect crystalline material has been proposed [Saka (2003). J. Appl. Cryst. 36 , 249–254]. In this method, the specimen was rotated around the scattering vector. By rotating the specimen, the integrated intensity of higher-order reflections was significantly increased from that in the initial vertical position. The results obtained were explained by assuming that the specimen was bent around an axis on the surface of the specimen, with the axis deviating slightly from the direction parallel to the edge of the specimen. In the present paper, it is shown that the results can be clearly explained by a model where the specimen is uniformly bent with a small torsion around the axes parallel to the specimen edges. The present model is highly probable, as the axes of the bending and torsion are parallel to the edges of the specimen.
    Type of Medium: Online Resource
    ISSN: 0021-8898
    RVK:
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2005
    detail.hit.zdb_id: 2020879-0
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  • 9
    Online Resource
    Online Resource
    International Union of Crystallography (IUCr) ; 2017
    In:  Acta Crystallographica Section A Foundations and Advances Vol. 73, No. 6 ( 2017-11-01), p. 474-479
    In: Acta Crystallographica Section A Foundations and Advances, International Union of Crystallography (IUCr), Vol. 73, No. 6 ( 2017-11-01), p. 474-479
    Abstract: Spherical wavefields in the Laue case are obtained when the real part of the crystal structure factor is zero or small compared with the imaginary part. The results are the same as in the conventional case where the real part is large. Through this work, it is shown that virtual wavefields on the vacuum side should be taken into account to explain the obtained results. It is also shown that, to obtain the virtual wavefields, a modification of the conventional spherical wave theory is necessary.
    Type of Medium: Online Resource
    ISSN: 2053-2733
    Language: Unknown
    Publisher: International Union of Crystallography (IUCr)
    Publication Date: 2017
    detail.hit.zdb_id: 2020844-3
    Location Call Number Limitation Availability
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