In:
Acta Crystallographica Section E Crystallographic Communications, International Union of Crystallography (IUCr), Vol. 73, No. 11 ( 2017-11-01), p. 1647-1651
Abstract:
The title compound, C 11 H 7 NS 2 , was prepared in high yield (87%) using a solvent-free microwave-assisted synthesis. The structure shows whole-molecule disorder with occupancies for two orientations (A and B) of 0.4884 (10) and 0.5116 (10), respectively. The thiophene and benzothiazole rings are almost planar and make dihedral angles of 10.02 (18) and 12.54 (19)° for orientations A and B, respectively. Slipped π–π stacking between the aromatic rings, together with C—H...π, C—H...S and C—H...N interactions, result in a herringbone motif in the crystal packing.
Type of Medium:
Online Resource
ISSN:
2056-9890
DOI:
10.1107/S2056989017014530
DOI:
10.1107/S2056989017014530/tx2001sup1.cif
DOI:
10.1107/S2056989017014530/tx2001Isup2.hkl
Language:
Unknown
Publisher:
International Union of Crystallography (IUCr)
Publication Date:
2017
detail.hit.zdb_id:
2843762-7
detail.hit.zdb_id:
2041947-8
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