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  • IOP Publishing  (2)
  • 1
    In: Materials Research Express, IOP Publishing, Vol. 7, No. 9 ( 2020-09-01), p. 095505-
    Abstract: Porous Ni–Cr–Mo–Cu alloys were fabricated by an activation reaction sintering technique with Ni, Cr, Mo, and Cu element powders as raw materials. The phase constitutes, morphology, and hydrogen evolution mechanism of the electrode were characterized by x-ray diffraction, scanning electron microscopy, and x-ray photoelectron spectroscopy. The electrochemical characterization for hydrogen evolution reaction (HER) was investigated by cyclic voltammetry curves, electrochemical impedance spectroscopy, and linear sweep voltammetry. Different parameters, including Cr content, temperature, and solution concentration that affected electrocatalytic activity for HER were also considered. The results illustrated that porous Ni–Cr–Mo–Cu electrodes possessed excellent hydrogen evolution performance, and the Cr content within a certain range 15 ∼ 25 wt% improved hydrogen evolution catalytic activity. The surface roughness R f of porous 60 wt%Ni-25 wt%Cr-10 wt%Mo-5 wt%Cu alloy electrodes was 8718.4, and the electrochemical activation energy is determined to be 7.46 kJ∙mol −1 , compared with 53.44 kJ∙mol −1 for porous 70 wt%Ni-15 wt%Cr-10 wt%Mo-5 wt%Cu alloy electrodes.
    Type of Medium: Online Resource
    ISSN: 2053-1591
    Language: Unknown
    Publisher: IOP Publishing
    Publication Date: 2020
    detail.hit.zdb_id: 2760382-9
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  • 2
    Online Resource
    Online Resource
    IOP Publishing ; 2022
    In:  Measurement Science and Technology Vol. 33, No. 10 ( 2022-10-01), p. 105006-
    In: Measurement Science and Technology, IOP Publishing, Vol. 33, No. 10 ( 2022-10-01), p. 105006-
    Abstract: Phase shifting laser interferometry is an effective method to measure the form error of a helical gear tooth flank. However, during measurement, part of the measurement light is inevitably shielded by an adjacent tooth or its own structure, and thus cannot be captured by the detector, resulting in the inability to collect a complete set of tooth surface shape information. This problem restrains the practicality of measuring a gear tooth flank by laser interferometry. We propose an analysis method and optimal search algorithm for shielding, to collect a complete set of tooth surface information from a measured gear. First, we propose an analysis method for shielding, based on ray-tracing, which allows the measurable region of helical gear tooth flanks with common parameters to be statistically analyzed. The variation law of the main parameters and a measurable region of the common helical gear tooth surface is expounded. Second, in order to obtain the complete interferogram, we propose an optimal search algorithm for shielding, by changing the relative position between the measured gear and the measurement optical system. Finally, relevant simulation and experiments prove that the proposed analysis and optimization methods are feasible. Furthermore, when the oblique incidence method is used to measure the shielded precision complex surface, the proposed methods of analyzing and optimizing shielding can be used for reference, to realize the complete measurement of the measured surface.
    Type of Medium: Online Resource
    ISSN: 0957-0233 , 1361-6501
    Language: Unknown
    Publisher: IOP Publishing
    Publication Date: 2022
    detail.hit.zdb_id: 1362523-8
    detail.hit.zdb_id: 1011901-2
    SSG: 11
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