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  • Blackwell Science Ltd  (2)
  • 1
    Electronic Resource
    Electronic Resource
    Oxford, UK : Blackwell Science Ltd
    Journal of oral rehabilitation 30 (2003), S. 0 
    ISSN: 1365-2842
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Medicine
    Notes: summary  This pilot study was undertaken to determine the compositional changes in tooth bleaching materials as a function of time in vivo. Ten patients were recruited and two bleaching systems were used – one a paste and the other a gel. Each material was placed in a custom bleaching tray and worn by each patient for each of four times – 15, 30, 60 and 120 min. The material was collected and chemically analysed for water by Karl Fischer titration and titrated for carbamide peroxide by the US Pharmacopoeia method. The paste material contained 18·66% water as supplied, and after 2 h this rose to between 28·6 and 64·4%. The gel material contained 2·85% water as supplied, and after 2 h this was diluted to between 28·5 and 73·4%. There was considerable difference in saliva uptake by the custom tray between patients. Most water uptake usually occurred within the first 30 min. Peroxide concentrations decreased in an approximately linear manner with time. There was a significant difference between the materials from baseline to 30 min and thereafter (P 〈 0·0009). This pilot study is an effective technique for chemical evaluation of bleaching materials. The effect of saliva is an important factor to consider, and is one that has hitherto not always been appropriately emphasized.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Oxford, UK : Blackwell Science Ltd
    Journal of oral rehabilitation 27 (2000), S. 0 
    ISSN: 1365-2842
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Medicine
    Notes: Tooth bleaching materials need to flow easily on insertion but should have high viscosity at low stresses to stay in place on the teeth. Some degree of elasticity may also aid retention on the teeth thereby maximizing efficacy. The present work was undertaken to study the comparative rheology of three tooth bleaching systems: two gels (Opalescence®, Ultradent; Perfecta Trio®, American Dental Hygienics) and a paste (Colgate Platinum®, Colgate). A dynamic stress rheometer (Rheometrics Scientific) with cone and plate geometry was used, with the materials maintained at 37·0±0·1 °C with a vapour hood to minimize volatilization. Stress creep and recovery experiments were carried out. Steady shear viscosity for all three systems was high (〉106 Pa s−1) for stresses 〈20 Pa. Between 100 and 200 Pa stress, all three materials showed a large drop in viscosity and flowed readily. The recovery portion of the data showed a marked difference where the elasticity of the gels was nearly two orders of magnitude higher than that of the paste. It was concluded that all materials would flow readily on insertion into the mouth and all have desirable high viscosity at low stress, but the paste material had the lowest elasticity. The effect of elasticity on performance needs to be determined clinically.
    Type of Medium: Electronic Resource
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