In:
Zeitschrift für Naturforschung B, Walter de Gruyter GmbH, Vol. 32, No. 10 ( 1977-10-1), p. 1215-1216
Abstract:
2-Methoxi-1,3,2-benzodioxastibole is prepared by transesterification of (CH 3 O) 3 Sb with catechol. Recrystallization from m ethanol yields colourless crystals, the structure of which was solved and refined to a conventional R-value of 0.04 with 915 reflections observed. The space group is P 2 1 /n with 4 molecules in the unit cell. Interaction with oxygen atoms of two neighbouring molecules enlarges the coordination number on the antimony to five, thus forming a structure with infinite chains along the α-axis.
Type of Medium:
Online Resource
ISSN:
1865-7117
,
0932-0776
DOI:
10.1515/znb-1977-1027
Language:
English
Publisher:
Walter de Gruyter GmbH
Publication Date:
1977
detail.hit.zdb_id:
2078109-X
detail.hit.zdb_id:
124635-5
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