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  • 2000-2004  (4)
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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 3846-3852 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The development and implementation of an all-optical technique for measuring thermal transport properties of materials at high pressure in a gem anvil cell are reported. Thermal transport properties are determined by propagating a thermal wave in a material subjected to high pressures, and measuring the temperature as a function of time using an optical sensor embedded downstream in the material. Optical beams are used to deposit energy and to measure the sensor temperature and replace the resistive heat source and the thermocouples of previous methods. This overcomes the problems introduced with pressure-induced resistance changes and the spatial limitations inherent in previous high-pressure experimentation. Consistent with the heat conduction equation, the material's specific heat, thermal conductivity, and thermal diffusivity (κ) determine the sensor's temperature rise and its temporal profile. The all-optical technique described focuses on room-temperature thermal properties but can easily be applied to a wide temperature range (77–600 K). Measurements of thermal transport properties at pressure up to 2.0 GPa are reported, although extension to much higher pressures are feasible. The thermal properties of NaCl, a commonly used material for high-pressure experiments are measured and shown to be consistent with those obtained using the traditional methods.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 77 (2000), S. 684-686 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The measurement of the temporal profile of the pressure in a shock wave propagating underwater and interacting with a nearby metal plate is presented. Pressures are deduced from the time-resolved fluorescence of a submillimeter ruby crystal mounted on an optical fiber tip. The measured pressures agree with finite-element code predictions, which model the production and propagation of the shock wave. These measurements are useful to evaluate shock-induced phenomena that are strongly dependent on the temporal profile of a shock wave, in small-scale testing, and in substantiating finite-element code predictions. © 2000 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 76 (2000), S. 2460-2462 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Experiments probing the dynamics of a thermal wave in a material compressed at static high pressures are presented. The method involves launching a thermal wave in a sample compressed in an anvil cell and monitoring the temporal profile of temperature at a fixed point downstream. A pulsed laser incident on a metal foil provides the thermal wave, while fluorescence from a small ruby sphere yields the time-resolved temperature. Results from compressed NaCl show that temperature rises quickly and decays much more slowly, consistent with the expected heat flow. This temporal profile evaluated with a numerical solution of the heat-conduction equation or an analytical approximation provides values for thermal conductivity, thermal diffusivity, and heat capacity at pressures to 1.7 GPa. © 2000 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    College Park, Md. : American Institute of Physics (AIP)
    The Journal of Chemical Physics 115 (2001), S. 1559-1564 
    ISSN: 1089-7690
    Source: AIP Digital Archive
    Topics: Physics , Chemistry and Pharmacology
    Notes: We have studied theoretically the effect of an external electric field on the equilibrium properties of lamellar and cylindrical assembly in confined diblock copolymers. The critical electric field at which a vertical morphology of lamellae is preferred over a horizontal configuration is found to have only a weak explicit dependence on the plate separation D when D is larger than a few bulk lamellar periods. In the case of the cylindrical morphology, the situation is found to be more complex, with the dimensions of the plates also playing a crucial factor. In both morphologies, the difference between the values of the polymer-plate interfacial tension for each of the two components is found to be a determining factor for the critical field. © 2001 American Institute of Physics.
    Type of Medium: Electronic Resource
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