In:
Journal of Materials Research, Springer Science and Business Media LLC, Vol. 14, No. 10 ( 1999-10), p. 3870-3872
Abstract:
A 100-nm CuFeS 2 ultrafine powder was prepared through a solvothermal reaction at 200–250 °C. X-ray powder diffraction and transmission electron microscopy results revealed that chalcopyrite-phase CuFeS 2 was crystallized with single-crystalline nature and preferential orientation growth. Mössbauer spectrum exhibited a six-peak hyperfine magnetic spectrum and a single nonmagnetic peak. Elemental analysis gave the atomic ratio of Cu:Fe:S of 1:1.02:2.10. The influence factors on the formation of CuFeS 2 ultrafine powder are discussed.
Type of Medium:
Online Resource
ISSN:
0884-2914
,
2044-5326
DOI:
10.1557/JMR.1999.0523
Language:
English
Publisher:
Springer Science and Business Media LLC
Publication Date:
1999
detail.hit.zdb_id:
54876-5
detail.hit.zdb_id:
2015297-8
Permalink