In:
Advanced Engineering Materials, Wiley, Vol. 24, No. 11 ( 2022-11)
Abstract:
Mo–Si–Ti alloys, like eutectic Mo–20Si–52.8Ti (at%), have previously been intensely investigated, owing to their excellent oxidation and creep resistance. To better understand high‐temperature mechanical behavior, a holistic assessment of microstructural features is necessary. Correspondingly, 3D‐focused ion beam tomography is carried out in Mo–20Si–52.8Ti. The results indicate a severely interconnected network of Mo solid solution (Mo SS ) and intermetallic (Ti,Mo) 5 Si 3 . Both phases retain similar network connectivity, lamellar sizes, etc. The brittle to ductile transition temperature (BDTT) is then determined through a series of bending tests and interpreted using the microstructural information. The BDTT is found to be ≈1100–1150 °C, different from Mo–9Si–8B with a continuous Mo SS network. The BDTT is an immediate consequence of the continuous network of both Mo SS and (Ti,Mo) 5 Si 3 . The Mo SS network is instrumental in crack trapping and bridging, indicating that the present phase distribution maximized the mechanical performance over (Ti,Mo) 5 Si 3 . Having determined the network microstructure and BDTT, tensile creep behavior is evaluated and compared to previously published compressive creep results. The results show consistency in terms of strain rate, stress exponent, and microstructural features indicating a reliably good creep resistance for the network microstructure of Mo–20Si–52.8Ti regardless of loading direction.
Type of Medium:
Online Resource
ISSN:
1438-1656
,
1527-2648
DOI:
10.1002/adem.202200918
Language:
English
Publisher:
Wiley
Publication Date:
2022
detail.hit.zdb_id:
2016980-2
detail.hit.zdb_id:
1496512-4
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