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  • Trans Tech Publications, Ltd.  (13)
  • Nie, Zuo Ren  (13)
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  • Trans Tech Publications, Ltd.  (13)
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  • 1
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2016
    In:  Materials Science Forum Vol. 877 ( 2016-11), p. 310-314
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 877 ( 2016-11), p. 310-314
    Abstract: To investigate the effect of cold-rolling and aging on precipitation and recrystallization behavior of Al-0.04Er-0.08Zr (at. %) alloy, two thermo-mechanical processes containing peak aging + cold-rolling ( A + CR ) and cold-rolling + isochronal aging ( CR + A ) were studied. In A + CR process, the hardness of alloy under cold-rolled state was much higher than the maximum obtained during isochronal aging, due to the strong interaction between precipitates and dislocations or sub-grain boundaries. Furthermore, the recrystallization temperature was 475 °C as indicated by the hardness curve. The microstructure analysis revealed that the sample annealed at 525 °C for 1 h still don’t recrystallize fully. For CR + A , it turned out that the deformation play a small role in improving the maximum of hardness. But comparing with those without deformation, the existence of deformation accelerated the rate of precipitation process and obtained higher electrical conductivity.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2016
    detail.hit.zdb_id: 2047372-2
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  • 2
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2016
    In:  Materials Science Forum Vol. 877 ( 2016-11), p. 514-521
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 877 ( 2016-11), p. 514-521
    Abstract: The Intergranular Corrosion (IGC) properties of Al-xMg-0.6Mn (x=3, 4, 5, 6 and 7) wt.% alloys were studied using the mass loss test. The mass loss test results of the alloys annealed at 100-300 ̊C for 1h indicated that the alloys with 3 and 4% Mg were resistant to IGC. While the mass loss values of the 6 and 7% Mg alloys were increased to IGC severe sensitive region, and then abruptly fallen to the IGC-resistant region with the increasing temperature. The mass loss-temperature curve of 5% Mg alloy was actually located between them. After isothermal annealing, the mass loss results indicated a stabilization temperature of the alloys with 5, 6 and 7% Mg appeared at the temperature beyond 220 ̊C, 250 ̊C and 270 ̊C, respectively. Furthermore, below the stabilization temperature 10-20 ̊C, it was observed a type of “special mass loss curve ” in so-called transition region that was showed a quick mass loss increasing to sensitization region and then a decrease to the IGC resistant region with a prolonged annealing time. To explore the “special curve” in transition region, the TEM observation of Al-7Mg alloy annealing at 250 ̊C was conducted, which indicated the sensitization resulted from the continuity of β phase, while the descending to the IGC might to be attributed to the spheroidization of β phase.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2016
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  • 3
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2016
    In:  Materials Science Forum Vol. 877 ( 2016-11), p. 303-309
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 877 ( 2016-11), p. 303-309
    Abstract: Effect of solution treatment on the properties and microstructural evolution of Al-Zn-Mg-Cu-Er-Zr alloy was investigated by hardness test, conductivity test, exfoliation corrosion test, scanning electron microscope (SEM), transmission electron microscopy (TEM). The results show that the hardness of single-stage solution treated samples first increase and then decrease, the conductivity and volume fraction of the residual phase particles decrease with increasing solution temperature. Compared to conventional multi-stage solution, slow heating process solution treatment can dissolve plenty of residual phases and further improve the hardness and decrease conductivity. Besides, the effect of solution treatment on EXCO is discussed, the result of exfoliation corrosion of SHT8 sample test is judged as EA. Moreover, the effect of the presence of nanometer-sized Al 3 (Er,Zr) particles on the microstructural evolution during solution treatment has also been discussed in detailed.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2016
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  • 4
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2015
    In:  Materials Science Forum Vol. 817 ( 2015-4), p. 399-405
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 817 ( 2015-4), p. 399-405
    Abstract: The effects of the homogenization conditions on the microstructure of Al-Zn-Mg-Cu-Zr-0.5Er alloy were investigated by differential scanning calorimetry (DSC), optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectrometry (EDS), and X-ray diffraction (XRD). The results showed that a lot of coarse phases existed in as-cast Al-Zn-Mg-Cu-Zr-0.5Er alloy. The dissolvable phases at grain boundary consisted of Mg 32 (Al, Zn) 49 . The residual phases dissolved into the matrix gradually during homogenization with increasing temperature and prolonging holding time. When the temperature increased to 465°C, and time prolongs to 24h, the main phase disappeared except the Fe and Er enriched phase, as a result of its high melting temperature. Taking into account the precipitation of Al 3 Er, we used a two-step homogenization .Hence, the optimum parameters of homogenization were 400 °C for 4 h and 465 °C for 24 h, which are good for the presence of coherent, elastically hard and nanosized Al 3 (Er, Zr) particles and the dissolvable coarse phases .
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2015
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  • 5
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2017
    In:  Materials Science Forum Vol. 898 ( 2017-6), p. 9-16
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 898 ( 2017-6), p. 9-16
    Abstract: The hot deformation behavior of aluminum alloy 5E61 was studied by hot compressive tests using a Gleeble-1500 thermal simulator. The tests were performed at temperatures varying from 250°C to 500°C and strain rates ranging from 0.001 s -1 to 10s -1 . The results achieved in the present study showed that the steady flow stress increases with decreasing temperature and increasing strain rate, in accordance with the Zener-Hollomon parameter. The related microstructure is sensitive to deformation temperature, strain rate and strain. The constitutive equation based on true stress-true strain curves has been developed by hyperbolic sine equation with the hot deformation activation energy of 153.907KJ/mol. The softening mechanism could be ascribed dominantly to dynamic recovery. The results of TEM observation suggested that Mn-containing particles and Al 3 (Er,Zr) phase have precipitated in the aluminum matrix and pin the dislocations, which could effectively inhibit the dynamic recrystallization.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2017
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  • 6
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2014
    In:  Materials Science Forum Vol. 794-796 ( 2014-6), p. 199-204
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 794-796 ( 2014-6), p. 199-204
    Abstract: The effect of heat treatment on the long-term corrosion resistance of Er containing 5083 aluminum alloy was studied using the micro-hardness test and mass loss test. The microstructure was analyzed by TEM. To maintain the strength, the annealing temperature was selected to be 100-230°C below the recrystallization onset temperature determined by the micro-hardness test. The plot of the annealing temperature versus the Intergranular Corrosion (IGC) initial time, which is determined by the Nitric Acid Mass Loss Test, showed a C-curve. The shortest IGC initial time (~1h) happened at 175°C, the nose temperature of the C-curve. When annealed at 125-200°C, the samples were IGC sensitive with the initial time less than 3h. The entirely IGC resistant (stabilized) samples were obtained when annealed at 220-230°C. The 175°C sensitized treatment was performed on the 220°C-stabilized samples, which showed that the 3-12h stabilization could significantly improve the resistance for long-term corrosion. TEM results showed that, for the IGC sensitive samples, β phases (Al 3 Mg 2 ) grew along the grain boundary continuously, while for the stabilized samples, they were isolated on triangle grain boundary and phase boundary.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2014
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  • 7
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2014
    In:  Materials Science Forum Vol. 794-796 ( 2014-6), p. 1044-1049
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 794-796 ( 2014-6), p. 1044-1049
    Abstract: The high temperature strength of aluminum can be improved by forming thermal stable precipitates of microalloying elements such as Er, Sc and Zr. Our previous research indicates that composite addition of Er and Zr can improve the amount of precipitations, but the aging time to approach the peak hardness is relatively long. In this paper, we will focus on the deformation behavior of the Al-Er-Zr alloy during hot deformation process and the corresponding microstructure evolution. The results show that the strain can induce rapid precipitation in Al-Er-Zr alloy during hot working conditions. The mechanism of the rapid precipitation and its effect on thermomechanical processing are discussed.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2014
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  • 8
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2017
    In:  Materials Science Forum Vol. 898 ( 2017-6), p. 29-34
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 898 ( 2017-6), p. 29-34
    Abstract: The microstructure of Al-6Mg-0.9Mn-0.07Zr-0.2Er (wt.%), registered as 5E61 alloy, were investigated using optical microscopy, scanning electron microscopy and transmission electron microscopy. The results showed that the addition of 0.2 wt.% Er can refine the dendritic structure and form fine and coherent L1 2 structured Al 3 (Er x Zr 1-x ) precipitates in the alloy. After a two-stage homogenization (280°C/10h, 460°C/36h), the recrystallization temperature of the alloy with 0.2 wt.% Er is about 15°C higher than that of the alloy without Er. The better recrystallization resistance may be related to the Al 3 (Er x Zr 1-x ) precipitates, which can pin on dislocations and sub-grain boundaries. The hardness of the cold-rolled alloy with 0.2 wt.% Er is 143HV, which is 5% higher than the alloy without Er. The exfoliation corrosion and nitric acid mass loss test were also performed. The exfoliation corrosion of the alloy is N grade, and the mass loss is only 9.84mg/cm 2 .
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2017
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  • 9
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2012
    In:  Materials Science Forum Vol. 706-709 ( 2012-1), p. 329-334
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 706-709 ( 2012-1), p. 329-334
    Abstract: Mechanical properties, corrosion resistance, and microstructure of Al alloys with trace element erbium were studied. Systemic studies in the pure aluminum and 5xxx series Al alloys showed that the tensile strength was significantly improved by above 20% with little loss of elongation by Er alloying. The 5xxx series Al alloys with erbium also exhibited excellent corrosion resistance. Erbium improved the aging hardness response of 7xxx series Al alloys and the addition of 0.4%Er to Al-Zn-Mg alloys increases the hardness by 35MPa. In all experiment Al alloys, a small addition of 0.1wt% Er induced a quick increase of the tensile strength and the amount of 0.4%Er shows optimized balance of the strength and ductility. The Er addition improved the thermal stability, with increasing the starting Rex temperature about 50°C in all investigated Al alloys. With regard to the microstructure mechanisms, in all experimental Al alloys Er addition has significantly refined the microstructure, which mainly attributed to presence the Al 3 Er particles. In the 7xxx series Al alloys, no observable PFZ after addition of 0.4% Er was found. The fatigue property, the fracture toughness and the thermal stability of microstructure and properties are on the way.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2012
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  • 10
    Online Resource
    Online Resource
    Trans Tech Publications, Ltd. ; 2020
    In:  Materials Science Forum Vol. 993 ( 2020-5), p. 116-122
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 993 ( 2020-5), p. 116-122
    Abstract: The hardness and microstructure of friction stir welded (FSW) 6082 aluminum alloy joint were investigated by Vickers microhardness test, optical microscopy (OM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). The hardness distribution is in a W shape, and from the base metal to the heat affected zone (HAZ) the hardness decreases from 103 HV to 72 HV, then gradually increases to 84 HV at the nugget zone (NZ). The grains of base metal (BM) are elongated and composed of a great quantity of low-angle grain boundaries. The nugget zon was of quite fine recrystallized grains. For the thermomechanical affected zone (TMAZ), the grain size is a little smaller than that of base metal and some low-angle grain boundaries remain. In the heat affected zone, the grain size was similar to that of the base metal. The β'' phase (Mg5Si6) and Al-Mn-Si particles are dispersed in the base metal. . In the heat affected zone, β'' phase transforms to β' phase (Mg9Si5). The hardness distribution in a W-shape was discussed on the basis of grain size, density of low-angle grain boundary and secondary phases.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2047372-2
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