GLORIA

GEOMAR Library Ocean Research Information Access

Your email was sent successfully. Check your inbox.

An error occurred while sending the email. Please try again.

Proceed reservation?

Export
Filter
  • Li, Shi Bin  (6)
  • 2020-2024  (6)
Material
Language
Years
  • 2020-2024  (6)
Year
  • 1
    In: Key Engineering Materials, Trans Tech Publications, Ltd., Vol. 861 ( 2020-9), p. 228-232
    Abstract: In this paper, the effect on the properties of alumina/aluminum cermet by changing the sintering temperature, and comparing the advantages and disadvantages of different characterization methods and their application range, it provides a reference for selecting the characterization technology suitable for alumina/aluminum composites.Through mixing, molding, sintering, sample preparation, scanning electron microscopic observation, energy spectrometer observation and analysis, the following conclusions can be drawn: the higher the vacuum sintering temperature, the more aluminum material is melted out of the body to form aluminum balls on the surface, and the green body The more severe the cracking. When the sample is sintered at a temperature of 600 °C, the density is the highest and the appearance is the best. When the molding pressure is 40 MPa and the sintering temperature is 700 °C, the microstructure of the sintered alumina/aluminum cermet is better. It can be seen from SEM and EDS analysis that the particles are continuously distributed and the larger one is metal Al, and the particles are discontinuously distributed and finer is Al 2 O 3 .
    Type of Medium: Online Resource
    ISSN: 1662-9795
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2073306-9
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 2
    In: Key Engineering Materials, Trans Tech Publications, Ltd., Vol. 861 ( 2020-9), p. 233-237
    Abstract: In this paper, the effect of sintering temperature on the interfacial structure of the composite was investigated and three different formulation groups were used to compare the respective properties. To obtain a composite material with excellent interface, the law between reference number and performance is obtained. Through mixing, molding, sintering, sample preparation, scanning electron microscopic observation, energy spectrometer observation and analysis, the following conclusions can be drawn: As the temperature increases, the density and hardness increase. The sample melts at 1500 °C, and there is no specific data. When the temperature reaches 1450 °C, the density and hardness reach the highest. When the formulation is Fe:Al 2 O 3 :SiO 2 =18:1:1 and the temperature reaches 1450 °C, the properties of the sample materials are optimized. The density is as high as 95% and the hardness reaches 42.9HBW.
    Type of Medium: Online Resource
    ISSN: 1662-9795
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2073306-9
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 3
    In: Key Engineering Materials, Trans Tech Publications, Ltd., Vol. 861 ( 2020-9), p. 289-294
    Abstract: Dye-sensitized solar cells have better development prospects than silicon cells, and their main structural composition of nanoporous semiconductor films is particularly important. It is the tin dioxide film, and the effect of preparing tin oxide film on dye-sensitized solar cells under different conditions is studied. In this paper, the SnO 2 powder was prepared by hydrothermal method, and the experiment was studied by controlled variable method. The properties of the obtained tin dioxide powder were characterized by SEM and three-dimensional ultra-depth microscope and XRD. The XRD diffraction peak is shown as tetragonal phase rutile type SnO 2 , With the increase of the concentration of tin tetrachloride solution, the coarser the particle size of the tin oxide crystal in the film, the more complicated the surface morphology, so that the specific surface area of the film is larger. At 0.1 mol/L, the surface of the film is a porous structure in the form of a loose sheet is presented. After analyzing the surface microstructure and flatness of the tin dioxide film, it can be concluded that the effect of salt concentration on the specific surface area of the film is extremely large. When the salt concentration is higher or lower, the obtained two the surface of the tin oxide film is relatively flat and has poor performance. When the salt concentration is 0.1mol/L, the surface of the obtained film has a large undulation and a large specific surface area, and the ability to adsorb the dye molecules can be predicted to be the greatest, and the photoelectric conversion efficiency is optimal in the photocatalytic process.
    Type of Medium: Online Resource
    ISSN: 1662-9795
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2073306-9
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 4
    In: Key Engineering Materials, Trans Tech Publications, Ltd., Vol. 858 ( 2020-8), p. 53-58
    Abstract: In this paper, the effect of raw materaisl on the properties of coated Al 2 O 3 /Al cermet materials were investigated, the raw materials were prepared via different methods, which provide a reference for obtaining higher performance cermet materials. Through mixing, molding, sintering, sample preparation, scanning electron microscopic observation, energy spectrometer observation and analysis, the following conclusions can be drawn, the density of the cermet material prepared by the mechanical ball milling method (83.5%) is higher than that of the cermet material prepared by the chemical precipitation method (92.8%). It is nearly 10% lower. The alumina particles prepared by the ball milling method are agglomerated, and a large amount of agglomeration occurs in the aluminum, and the composition is very uneven. For materials prepared by the precipitation method, the aluminum oxide is uniformly distributed in the aluminum. The ball-milling powder is used to prepare materials, most of the alumina is in the form of particles, and in the precipitation method. In the powder preparation sample, the thin layer of alumina which forms the same eggshell envelops the aluminum, and the aluminum has a certain liquid phase change. the surface hardness (824HV) of the cermet material prepared by the mechanical ball milling method is lower than the surface hardness (1005HV) of the cermet material prepared by the chemical precipitation method.
    Type of Medium: Online Resource
    ISSN: 1662-9795
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2073306-9
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 5
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 977 ( 2020-2), p. 72-77
    Abstract: Nano-SnO 2 is a relatively important semiconductor material. Its crystal structure is unique rutile type. It has the advantages of high conductivity, high transparency and stable chemical properties. It is widely used in gas sensing detectors and solar cells for photoelectric conversion. Applications. In this paper, SnO 2 nanofilms with different crystal structures were prepared by changing the three process parameters of salt concentration, reaction time and hydrothermal temperature in hydrothermal method. The samples were tested by scanning electron microscopy (SEM) and three-dimensional ultra-depth microscopy analyzer. As the concentration of the reaction solution increases, the macroscopic thickness of the film gradually thickens, and the three-dimensional structure of the surface changes from flat to coarse to coarse peak. The peak between the peaks first increases and then decreases, and the surface microstructure is The conditions change are not obvious. Through the comprehensive comparison of film integrity and surface area, it is found that the concentration is 0.03mol/L, which is relatively better.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2047372-2
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
  • 6
    In: Materials Science Forum, Trans Tech Publications, Ltd., Vol. 977 ( 2020-2), p. 96-101
    Abstract: Both alumina and boron carbide have good hardness and strength, and are widely used in production and life, industrial manufacturing, and military defense. However, due to the insufficiency of research at this stage and the lack of technical means, it is difficult to prepare alumina-boron carbide composite powder with good coating and ultra high strength through large-scale batch production. Therefore, this experiment wants to obtain a relatively good performance of coated Al 2 O 3 /B 4 C cermet by hydrothermal method through different experimental parameter ratios. Through the experimental results and analysis, the following conclusions are obtained. The most suitable concentration of aluminum nitrate is 0.1 mol/l. The low concentration affects the formation of alumina particles. The concentration is too high and prone to agglomeration. Through the optimization of hydrothermal synthesis concentration, a composite of Al 2 O 3 /B 4 C composite with good nanoencapsulated structure was obtained. The composite powder was pure in composition and high in specific surface area, which lays a foundation for solving the low-temperature preparation of high-density boron carbide ceramics.
    Type of Medium: Online Resource
    ISSN: 1662-9752
    URL: Issue
    Language: Unknown
    Publisher: Trans Tech Publications, Ltd.
    Publication Date: 2020
    detail.hit.zdb_id: 2047372-2
    Location Call Number Limitation Availability
    BibTip Others were also interested in ...
Close ⊗
This website uses cookies and the analysis tool Matomo. More information can be found here...