In:
Powder Diffraction, Cambridge University Press (CUP), Vol. 35, No. 2 ( 2020-06), p. 124-128
Abstract:
X-ray powder diffraction data for new metal-organic compounds: tetrakis(3-ethylanilinium) octamolybdate Mo 8 O 26 (C 8 H 12 N) 4 [ a = 10.682(4), b = 16.589(5), c = 7.307(2) Å, α = 92.79(2)°, β = 97.99(3)°, γ = 103.89(3)°, V = 1240.27 Å 3 , Z = 1, space group P− 1]; tetrakis(3-ethylanilinium) octamolybdate tetrahydrate Mo 8 O 26 (C 8 H 12 N) 4 ·(H 2 O) 4 [ a = 18.801(7), b = 17.943(6), c = 7.334(3) Å, β = 98.50(5)°, V = 2446.99 Å 3 , Z = 2, space group P 2 1 / m ] and bis(3-ethylanilinium) pentamolybdate Mo 5 O 16 (C 8 H 12 N) 2 [ a = 34.643(6), b = 5.5796(7), c = 14.200(3) Å, β = 96.20(2)°, V = 2728.69 Å 3 , Z = 4, space group I 2 /a ] are reported in this paper. The investigated compounds were synthesized from molybdic acid and 3-ethylaniline in acidic solution. In the first two cases, we obtained octamolybdates, while the last compound crystallized as pentamolybdate.
Type of Medium:
Online Resource
ISSN:
0885-7156
,
1945-7413
DOI:
10.1017/S0885715620000123
Language:
English
Publisher:
Cambridge University Press (CUP)
Publication Date:
2020
detail.hit.zdb_id:
2047596-2
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