In:
Review of Scientific Instruments, AIP Publishing, Vol. 79, No. 9 ( 2008-09-01)
Abstract:
The electrophoretic mobility, which reflects the zeta potential of a solid material, is an important experimental quantity providing information about the electrical double layer at the solid/liquid interface. A new high temperature electrophoresis cell was developed suitable for electrophoretic mobility measurements of dispersed nanosize particles up to 150 °C and 40 bars. Amorphous silica (SiO2) particle size standards were used to test the particle size detection limit of the new instrument at 25, 100, and 150 °C and several pH values. The microscopic detection of the particles was enabled by dark-field illumination, which allowed extending the previously available capabilities and provided higher accuracy of the electrophoretic mobility data. The electrophoretic mobility measurements for SiO2 at temperatures above 100 °C were reported for the first time and indicated a gradual increase in particle electrophoretic response with increasing temperature. The obtained data indicated negatively charged SiO2 surface throughout the pH and temperature ranges studied.
Type of Medium:
Online Resource
ISSN:
0034-6748
,
1089-7623
Language:
English
Publisher:
AIP Publishing
Publication Date:
2008
detail.hit.zdb_id:
209865-9
detail.hit.zdb_id:
1472905-2
SSG:
11
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